GCMS analysis results for sample AE03250, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 . Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L * ******************************************************************** Peak Number 7 3-Buten-2-ol, 2-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.15 ug/L 74670 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 2 Butenol, methyl- 86 C5H10O 060766-00-9 72 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 4 3-Buten-2-ol, 2-methyl- $$ .alph... 86 C5H10O 000115-18-4 64 Abundance Scan 146 (5.022 min): 03250.D (-) m/ z 71.10 100.00% 43 71

5000

li 50 I i 55 59

67 \ Ny 4 4.60 4.80 5.00 5.20 5.40 — 1 86 m/z 43.10 95.03% Oh III 11'11 ■ i' " ■ i11'11 ■1 " i ■ ' " r ■ " i' " 111 " ' i " " i n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4084: 3-Buten-2-ol, 2-methyl- 71 43

5000 . A/Ay/ r A A. 59 4.60 4.80 5.00 5.20 5.40 m/z 41.10 58.66% 27 53 67 86 PIPPmPTTT — —H '1 ■ i " 11 r " ' H 11 ■ r 1 ■' i n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4093: Butenol, methyl- 43 71 N 4.60 4.80 5.00 MAAA A 5.20 5.40 5000 59 m/z 69.10 46.45% 27 15 31 53 Or5 ■ ■ i" mH H "r " 'i■ ‘IT 67 ,...... 86 " i " " i'1 1 " i " '111" ' i111' i “ " i m/z- > Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #4083:3-Buten-2-ol, 2-methyl- 71 0 4.60 4.80 5.00 5.20 5.40 43 m/z 59.00 42.41%

5000 59 27 31 53 °b5 10 15 20 25 ‘ 30T 3537 -H 1............... ............... '' i " '' r ''11' ■ ■ ■ i1 A A N m/z-> 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

33250.D HP022102.M Mon Mar 04 12:33:41 2002 Page 9

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