GCMS analysis results for sample AE00108, Feb 2002

NYC 9/11 Public Portal Document 2 wUIp/tl.ti A\SMVA L

Data File : C:\MSDCHEM\1\5973N\O2JAN25\00108.D Vial: 6 • Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Buten-2-ol, 2-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.24 ug/L 108168 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 86 2 Butenol, methyl- 86 C5H10O 060766-00-9 80 3 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 78 4 3-Buten-2-ol, 2-methyl- $$ .alph... 86 C5H10O 000115-18-4 72 Abundance Scan 143 (5.006 min): 00108. D (-) m/z 71.10 100.00% 43 71

5000 59 39 53 -AA A. I \ . 4.60 4.80 5.00 5.20 5.40 TTTTT — 85 " ।" i ■u • i ‘ ‘ 11u 111" " । ■ -TmPTTTTT m/ z 43.10 87.77% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4083:3-Buten-2-ol, 2-methyl- 71 43

5000 LAA/-A— 59 4.60 4.80 5.00 5.20 5.40 27 31 m/z 41.05 50.21% 53

n/z—> 5 '11"111 H ' ■ i" ■111 -4. 37 — -HH mPH 10 15 20253035404550556065 70 75 808590 ,............... 86..........

Abundance #4093: Butenol, methyl- 43 7h A.. N AAAAA— m/z 4.80 4.60 5.00 59.10 5.20 5.40 40.54% 5000 59 27 15 31 53

m/z-> 5 '11 “ ’ ’I’*’’’ ’IT ’ ’1’141111 10 15 20 25 30 35 40 45 50 55 60 65 m —7+70 75 80 85 90 , 86 1 n r ■" i'1" I" " 11"11

Abundance #4081:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 71 +4 P. AA r.5.00 ■ 4.60 4.80 5.20 5.40 m/z 69.10 39.25% 43 5000 59 2731 53 9 । 67 pmpm TT 1 "I" ml Tp-r > ■ । ■ 11 > | n 1111 ■ >! । > 1111 ................................ -TTIPPTT n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

30108.D SCAN508.M Mon Jan 28 09:49:59 2002 Page 7

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