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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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Data File : C:\MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 • Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Insttumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************* * * Peak Number 6 l-Hexene, 4,5-dimethyl- $$ ... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.71 0.16 ug/L 70128 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# : Qual l l-Hexene, 4,5-dimethyl- $$ 4,5-D... 112 C8H16 016106-59-5 59 2 3-Buten-2~61, 2-methyl- 86 C5H10O 000115-18-4 43 3 3-Penten-2-ol $$ .alpha.,.gamma.... 86 C5H10O 001569-50-2 42 4 3 -[.beta.-hydroxy-(.beta.,■beta .. 86 C5H6D2O 005557-87-9 38 Abundance Scan 205 (5.714 min): 00108.D (-) m/z 71.10 100.00% 41 71

5000 45 TT 53 58 — 5.40 5.60 5.80 6.00 m/z-> I' ‘ " I 14941,.4.7..67 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 84 1111" 111' ■ 11''111M •1111 ■11 ■' " i m/ z 41.10 98.10% Abundance #13811:1-Hexene, 4,5-dimethyl- $$ 4,5-Dimethyl-1-hexene 43 71

5000 39 55 _.,.5.40 +. 5.60/N l, 5.80 TT 6.00 27 m/z 43.10 :91.43%

■nfe-> i ■"' i m L - 67 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 .. A4.. 97.. Abundance #4085:3-Buten-2-ol, 2-methyl- 43 7 * /Y. । 1, I i , । 5.40 5.60 5.80 6.00 5000 m/z 69.10 43.15% 59 27 31 53

iz-> ' ■ r 1" r TTT +-4+7+" iH " i 86 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 '"i1"'P " ' i1" ■ i" "i"'1111 u i1

Abundance #4047:3-Penten-2-ol $$ alpha., gamma.-Dimethylallyl alco... . pn.। 43 71 5.40 5.60 5.80 6.00 m/z 39.10 40.75% 5000 39 27 53 67 58 86

n/z-> 11 H 11 '.mll +r 49 TT’" Tp-r • | * ’ * 'lii* 1 I ‘ * • I « । ■ > I '. PPTP ■ । | ‘ ri । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 5.40 5.60 5.80 6.00

50108.D SCAN508.M Mon Jan 28 09:49:59 2002 Page 8

NYC-WTC_000050765

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NYC-WTC_000050765Source: NYC Law Department, mirrored locally

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