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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/24 - 1/25/02
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GCMS analysis results for sample AE00250, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.

NYC-WTC_000050596–000050614

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050607
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN24\00250.D Vial: 6 . Acq On : 24 Jan 2002 7:06 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 1,6-Heptadien-4-ol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 5.71 0.25 ug/L 121071 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 53 2 3- [.beta.-hydroxy-(.beta.,.beta.... 86 C5H6D2O 005557-87-9 53 3 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 50 4 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 46 Abundance Scan 205 (5.714 min): 00250.D (-) m/z 71.10 100.00% 43 71

5000 .... A... 84 53 58 5.40 5.60 5.80 6.00 3 +mHmlmH ------- i . < ■ । > > i i । i . > < ।. I . i । . 11 11 H i i | . 111 [ m/z 43.10 93.73%

L nz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #13655:1,6-Heptadien-4-ol 43 71

5000 ----- 5.40 5.60 5.80 6.00 27 m/z 41.10 85.32% ,.. 15.11 .. 66,1, , 79 84 94 1112221113201300100001100011228317 T-rp-rrrj-rrr T‘ n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3392:3-[.beta.-hydroxy-(.beta.,.beta.-dideuterio)]ethylp... Th . 1 > l ■ BI4f4T T ’l ■ L IT 11 I' 5.40 5.60 5.80 6.00 5000 m/z 69.10 38.57% 58 85 44 53 ■ I > ■ | I I I I | I > 11 | l I 1 I | ■ 11 > [ ITI I | I mmHir | । • । । 11 ■ 164 mpp miz—> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #4043:3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 43 71 A ' ‘ ' I 1 1 ‘ 1 I ‘ ‘ 1 ' I ‘ 5.40 5.60 5.80 ‘ ' I ‘ 6.00 ‘ I

m/z 39.10 38.40% 50)0 27 15 53 58 86

miz—> -LP.7 -TH —mmmpmpmt ■‘‘‘i■••■i■ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 5.40 5.60 5.80 6.00

00250.D SCAN508.M Fri Jan 25 10:26:23 2002 Page 8

NYC-WTC_000050607

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NYC-WTC_000050607Source: NYC Law Department, mirrored locally

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