GCMS results for sample AE00697, Jan 29 2002

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN16\00697.D Vial: 3 . Acq On : 16 Jan 2002 12:31 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 2-Pentyn-l-ol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 4.85 0.18 ug/L 58411 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentyn-l-ol 84 C5H80 006261-22-9 35 2 2,3,4,5-Tetrahydropyridazine 84 C4H8N2 000694-06-4 32 3 4-Pentenal (CAS) $$ 4-Pentenal- 84 C5H8O 002100-17-6 9 4 1-Hexene, 6-bromo-____________________ 162 C6HllBr 002695-47-8 9 Abundance Scan 129 (4.846 min): 00697.D (-) m/z 84.10 100.00% 84

55 59 5000 41

MRMAAAYMWA "B7

miz-> Ol - ■ i ' 1 । ' I > 20 25 । > i ■ ■ • । I 30 35 A40 45 51

50 55 i '' ' ' i ■ ■ ■ • i ■ ' ■ ■ i 1 • ■ 1 i' ' 60 65 70 75 80 TTT" 1 I 1 ' 85 90 4.60 4.80 5.00 5.20 4.40 m/z 55.10 52.32% Abundance #3292:2-Pentyn-1-ol 39 55

83 5000 27 4 40 4.60 4.80 5.00 5.20 51 m/z 59.00 47.66% 69 n/z-> 01 " i ' 1 ' 1 i ‘ 20 ′′′′′′′′′ ----- — 25 30 35 40 45 50 55 60 —65L 65 70 "IT 75 80 85 90 Abundance #3177:2,3,4,5-T etrahydropyridazine 84 0 29 4.40 4.60 4.80 5.00 5.20 5000- 55 m/z 41.10 44.02% 41 26 69 44 - ol n/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 ■11 ■ ■ ■11' ■

#3208: 4-Pentenal (CAS) $$ 4-Pentenal- 41 55 i11'' i' ■ ■ ■ i'' 80 85 90 _LL 4.40 4.60 4.80 5.00 TTFTT 5.20 m/z 39.10 40.66% 5000

83 44 51 58 69 ............................................

m/z-> 0 ■ ■ i ■'1 11 "TTTI 11111111 20 25 30 35 40 45 50 55 60 65 T... ml,... 70 75 80 85 90 4.40 4.60 4.80 5.00 5.20

)0697.D SCAN508.M Thu Jan 17 08:16:54 2002 Page 3

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