GCMS surrogate recovery results for sample AE00277, Jan 2002

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\l\5973N\02JAN09\277.D Vial: 2 Acq On 9 Jan 2002 6:59 pm Operator: Sample 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 3-PENTEN-2-OL, (Z)- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.11 ug/L 49353 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-PENTEN-2-OL, (Z) - 86 C5H10O 024652-50-4 35 2 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 35 3 3-Penten-2-ol 86 C5H10O 001569-50-2 35 4 3-Penten-2-ol $$ .alphagamma .... 86 C5H10O 001569-50-2 30 Abundance Scan 143 (5.006 min): 277.D (-) m/z 71.05 100.00% 43 71

5000 39 55 59 A_ 84

n/z-> 49 1 1 01 "I" - 1 I " " I " '1 111 " I " 20 25 30 35 40 45 50 55 60 65 70 75 80 85 m90 95 4.60 m/z 4.80 43.05 5.00 5.20 5.40 95.61% Abundance #4208: 3-PENTEN-2-OL, (Z)- 71 43

5000' 39 53 67 AAAAAAla 4 60 4.80 5.00 5.20 5.40 27 m/z 69.10 75.69%

n/z-> 01 ■' i'T'' i' TPPTTH + 58 ■ i> • > ■ i > • ■ > i ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 I90 95 86

Abundance #4045: 3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 71 A - 43 4.60 4.80 5.00 5.20 5.40 5000 m/ z 41.10 69.80%

53 58 67 86

Tl/Z—> Abundance 16 01 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ • ■ • । • • ■ ■ । ■ I ' I' ■ ■11' --HH —TIT - 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

43 #4046: 3-Penten-2-ol 71 ANAy. 4 60 m/z 4.80 59.10 5.00 5.20 5.40 41.39%

5000 39 53 67 27 58 86

/z-> 0 ■■i■■■■i ■ 20 25 ■' i M111 ■ । ‘ 30 35 40 45 ‘IT I J... 50 55 60 65 "UI I 70 75 80 85 90 95 A 4.60 4.80 Apeppreept 5.00 5.20 5.40

277.D SCAN508.M Thu Jan 10 11:51:37 2002 Page 7

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