GCMS analysis results for sample AE00470, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00470.D Vial: 4 Acq On : 15 Jan 2002 12:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 4 3-Buten-2-ol, 2-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 5.71 0.16 ug/L 51308 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 59 2 3-Penten-2-oL (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 45 3 3-Penten-2-ol 86 C5H10O 001569-50-2 42 4 3-Buten-2-ol, 2-methyl-__________________ 86 C5H10O 000115-18-4 42 Abundance Scan 205 (5.714 min): 00470.D (-) m/z 71.10 100.00% 43 7h

5000 39 ' 5.40 5.60 ^5.80 665" ' ' 51 58

/z-> 5 01 rl" " I' i " ■' i " " r mmT .I.... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 84 m/z 43.10 87.87% Abundance #4085: 3-Buten-2-ol, 2-methyl- ■ ■ i 1 . | . . । 71 43

5000 59 5.40 5.60 5.80 6.00 27 31 m/ z 41.10 80.23%

m/z-> 0 5 1 ■ i " " i " '11' " ' r ‘IT "i " " i " + -H 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 53 671 86 I । | | | i | i ! >-ri i Tmme

Abundance #4043: 3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... 43 7 ‘ ' 1 I ' TTT 5.40 5.60 5.80 6.00 5000 27 m/z 69.00 46.18% 15 53 3158 67 86

/z-> Of 5 11111 5 '111" ' r • I ■ । 1111 • ■ < । ■ 1 ■ I +Trri ■' I ■ 11 ■ 11 ■ >«111 > 11 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 i-ryT t

Abundance #4042: 3-Penten-2-ol . r non 4 Mo 71 5.40 5.60 5.80 6.00 43 m/z 39.10 36.06% 5000

27 53 58 86 67 - iz-> Or 5 ............................ | 37 ■11 ’1 ■11 ■11111 ■ ■1111111" 1111111111 H -H++ *mmmPP 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.40 5.60 5.80 6.00

00470.D SCAN508.M Wed Jan 16 08:13:51 2002 Page 6

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