GCMS analysis results for sample AE00470, Jan 2002

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Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.

NYC-WTC_000051697–000051713

Folder label: “GCMS X 1/9/02 A 1/15/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00470.D Vial: 4 Acq On : 15 Jan 2002 12 :42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 Silane, tetramethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.77 ug/L 1223100 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 38 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 3 -(CYCLOHEX-3'-EN-YL)PROPANOL $$. . . 174 C8H14O4 015745-87-6 33 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 28 Abundance Scan 220 (5.885 min): 00470. D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 01 ' r ' " i' " ■ i ■' ■ 'TI 11I'' ■ ------- 55 ,i, 87 103 m/z 43.10 25.26% i ‘ ‘‘I ''11 r1'111 ■■ ■11 ■ । ■ h ■" ' i ■ " 11" '1111111'1111' " 11'' " r 11' i' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 7)3 _ . • ( i r। । । i । ।

5000 5.60 5.80 6.00 6.20 m/z 45.10 9.67% 45 15 | 53 1 1 i ' _ * > । ri o1 T’T I '' ■ ■ I THTt TI‘—n—88 uu0me—09*—n—nemOOT—mopr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.32%

43 27 o1 ' I'1'111 Tr 1 r55■ " i " ■ ■ I' ", " i "87i'1" i " " H3 i""r"'i""i ।1'' ■ । 174 i'1'' i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7)3 5.60 5.80 6.00 6.20 m/z 71.10 6.80%

5000

m/z-> 27 + 0 '"i" "I"'1........... .... . ■ i ■ 55 , I p-r-rrp 87

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 113 | 11 i i | i i r ■ । r . i i । I' ■ I 174 -4.. , 5.60 5.80 6.00 6.20

00470.D SCAN508.M Wed Jan 16 08:13:51 2002 Page 7

NYC-WTC_000051707

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