NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN15\00559.D Vial: 3
Acq Cn : 15 Jan 2002 3:10 pm Operator:
Sample : 508 scan Inst : Instrumen
Mise : January 15, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator)
Title : 508 scan method
Library- : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 3 Silane, tetramethyl- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.89 4.26 ug/L 1315740 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 43
2 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 36
3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33
4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33
Abundance Scan 220 (5.885 min): 00559.D (-) m/ z 73.10 100.00%
73
5000
43
5 60 5.80 6.00 6.20
I । 55 . 87 103
0-7 -PP 1IPHPUTTUTTT i1 " ' i' m/z 43.10 23.87%
m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180
Abundance #4814: Silane, tetramethyl-
73
-----
5000
5.60 5.80 6.00 6.20
m/z 41.10 9.72%
45
15 | 88| 53
0 TTmPTTTTm TTr-p-rr-rj- I " " I " " I " " I " " r " ' i "'' i T‘
n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1 50 160 170 180
Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p...
73
. . r ......
5.60 5.80 6.00 6.20
5000 m/z 45.10 9.01%
L
55 87
27 45
0 j__ L — i... TCP’ I "11111" i " i' TT v
n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180
Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... ‘‘ I’’
73 5.60 5.80 6.00 6.20
m/ z 71.10 6.56%
5000
43
m/z->
27
0 -- --PT
55 . 87
+ 113 174
1111' I " " i11'1111" i ■ " ■i'1■ ■ i ■ " ' i ■1" i■1■■ i ■
10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180
.........
5.60 5.80 6.00 6.20
00559.D SCAN508.M Wed Jan 16 08:14:05 2002 Page 5
NYC-WTC_000051735
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