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GCMS analysis results for sample AE00559, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.

NYC-WTC_000051727–000051739

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051735
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00559.D Vial: 3 Acq Cn : 15 Jan 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.26 ug/L 1315740 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 43 2 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 36 3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 Abundance Scan 220 (5.885 min): 00559.D (-) m/ z 73.10 100.00% 73

5000

43 5 60 5.80 6.00 6.20 I । 55 . 87 103 0-7 -PP 1IPHPUTTUTTT i1 " ' i' m/z 43.10 23.87% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73

----- 5000 5.60 5.80 6.00 6.20 m/z 41.10 9.72% 45 15 | 88| 53 0 TTmPTTTTm TTr-p-rr-rj- I " " I " " I " " I " " r " ' i "'' i T‘ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1 50 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73 . . r ...... 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.01%

L 55 87 27 45 0 j__ L — i... TCP’ I "11111" i " i' TT v n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... ‘‘ I’’ 73 5.60 5.80 6.00 6.20 m/ z 71.10 6.56% 5000

43

m/z-> 27 0 -- --PT 55 . 87 + 113 174 1111' I " " i11'1111" i ■ " ■i'1■ ■ i ■ " ' i ■1" i■1■■ i ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ......... 5.60 5.80 6.00 6.20

00559.D SCAN508.M Wed Jan 16 08:14:05 2002 Page 5

NYC-WTC_000051735

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NYC-WTC_000051735Source: NYC Law Department, mirrored locally

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