GCMS analysis results for sample AE03248, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial : 3 . Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 3-Buten-2-ol, 2-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.09 ug/L 43056 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 53 2 3-[.beta.-hydroxy-(.beta.,.beta.... 86 C5H6D20 005557-87-9 47 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 42 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 42 Abundance Scan 145 (5.011 min): 03248.D (-) m/ z 43.10 100.00% 43 71

5000 59

I 49 I 55

84 IMAWMAAA । ■ ■ ■ 1 i..... 11 1 1 । 4.60 4.80 5.00 5.20 1 1 । 1 1 5.40

m/z-> 01 . J- ana—— 20 25 30 35 40 45 50 55 - 60 65 70 - 75 80 85 90 95 m/ z 71.10 88.83% Abundance #4085: 3-Buten-2-ol, 2-methyl-

5000

27 31 43

59 71

4.60 m/z i. 4.80 41.10 5.00 5.20 5.40 49.10% 67 । 86 O+ T’T ' ■ i' 1 '1 i1 ' +Tt - '1 ■ i' " 11'''' i1 ■ " i " '' i n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance

5000 #3392: 3-[.beta.-hydroxy-(.beta.,.beta.-dideuterio)]ethylp... 71 th M /.. 4.60 m/z 4.80 59.10 5.00 5.20 5.40 46.51% 58 85 68 53 44 Ot----- -rp-r ‘It ■ ।11" ।11 1 I I m/z-> ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4084:3-Buten-2-ol, 2-methyl- N. IBB 0 71 4.60 4.80 5.00 5.20 5.40 43 m/z 69.10 42.45%

5000 59

27

n/z-> 0 m 20 25 30 35 40 50 53 TIT 11111111111' '"t I " 111111 45 55 60 67

65 70 — ■ ■ ■ 11 ■ ■ ■ । ■r ■ ■ । 75 80 86

85 90 95 4.60 4.80 5.00 5.20 5.40

3248.D HP022102.M Mon Mar 04 12:33:27 2002 Page 7

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