GCMS analysis results for sample AE03248, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03248 conducted on March 15, 2002.

NYC-WTC_000006146–000006165

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 . Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.75 ug/L 2203380 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 Abundance Scan 223 (5.891 min): 03248.D (-) m/z 73.10 100.00% 73

5000 43 1111/’ 11 ‘ I’’*’ 5.60 5.80 6.00 6.20 ............ 11.55... J 87 [ . . . I |103I . I I M | | I t t I ( T-: >1 | I I I I [ I I I I | ■ I I I | I I I I ] ) o1'' I'' " I' " ' I ‘" 11,1' I'1'11''' 11 ।rge .-l'l m/ z 43.05 22.97% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 ■ । 1 i ■ .■ — , t । ■ । '■ i , । . 5.60 5.80 6.00 6.20

C 43 m/z :45.10 9.24% 27 87 113 55 .1 , 174 0- 1111' " i111' r 1'11'111' i i " 11 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/ z ■41.10 8.68% 43 27 0-T 55 87 I I/’l......'.........'I1'1 , 113 174 " i'1 " i " " 111111" " I " " I " " 11 1" i " 1' i " '' i ■ " 11 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 11t 1 ' 1 T r ' 1 11in T | > , I-. 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.08%

5000 44 58 15 m/z-> 0- melijunn TTTTTTTLUTTTTTTTTTTTTTTTTTLTTTTTTTTTTIWIPTIWTPTTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

33248.D HP022102.M Mon Mar 04 12:33:28 2002 Page 8

NYC-WTC_000006157

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GCMS analysis results for sample AE03245, March 2002 · Box DEP Box 12

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

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