Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.
NYC-WTC_000050856–000050874Folder label: “GCMS X 1/7/02 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN09\278.D Vial: 3 Acq On 9 Jan 2002 7:50 pm Operator: • Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.89 4.45 ug/L 2186350 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3 -(CYCLOHEX-3 ′ -EN-YL)PROPANOL $$ . . . 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 32 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 278. D (-) m/ z 73.10 100.00% 73
5000 43 ' 1 i 1 1 1 ' i 1 1r-r-r-pr-r-r-r-p-r 5.60 5.80 6.00 6.20
m/z-> O'* ■ । । l । ■ 111 > 55 11 , ■ ■ r '87 TT’TTTgT 103 ■ i ■ ■ ■ ■ i ■' ■ ■ i " ■ ■ i ''■ i' ■ ■' i t
10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.10 25.18% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70
5000 1 1 I ' 1 ' I ' ' ' ' I 1" 1 I ' ' 5.60 5.80 6.00 6.20 43 m/z 45.10 9.49% 27 55 113 87 174 01 TTTTTTTTTTTTT TTT i .। ’ 0’ I ' r ■ ■ ■ i ■ ■ ■ ■ r ' " r " ' i TTTIn m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70 —TRAr 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.11%
n/z-> Abundance
5000- 0 -IPP 27 55 Tmm 43 . P87 113 r " ' i " " r 1'11 ■ ■ " r ■ •' r " • i ■ " ' r ■ " i'11111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #4813: Silane, tetramethyl- (CAS) $$ Tetramethylsilane $$ ... 70 174
t1Td 5.60 m/ z 71.10 1 5.80 6.00 *TTrrr 6.20 6.83%
45 15 31। 53 | 88 0 '' r ■ " i' " 11 ■ r i i । I Pl i । 1111] >r'i'i""i"’' i’"• i "■' i"• • i ’ "' i■ ■ ••i■■■'i■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
278.D SCAN508.M Thu Jan 10 11:51:44 2002 Page 5
NYC-WTC_000050865
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050932
Laboratory record documenting GCMS surrogate recovery data for sample AE00282 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050875
Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051685
Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051727
Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050963
Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051755
GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050977
Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051714
Laboratory report showing GCMS analysis results for sample AE00558 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050813
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050814
Fragmented page from a DEP laboratory record showing method parameters and sample data fields for January 7-9, 2002 testing.
Filed in the same folder
NYC-WTC_000050817
Technical form detailing GCMS analysis results for sample AE00277 listing detected compounds and concentrations from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050821
Reference report for GCMS analysis of sample AE00277 listing compound names and qualifier values from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
Filed in the same folder