GCMS analysis results for sample AE03248, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 . Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Hexanamide $$ n-Caproamide ... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.88 0.06 ug/L 28360 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexanamide $$ n-Caproamide $$ n-... 115 C6H13NO 000628-02-4 9 2 3-Butenoic acid $$ . beta.-Buteno. . . 86 C4H602 000625-38-7 7 3 3-Butenoic acid (CAS) $$ Vinylac... 86 C4H602 000625-38-7 7 4 Formamide, N-methyl- (CAS) $$ N-... 59 C2H5NO 000123-39-7 4 Abundance Scan 576 (9.876 min): 03248.D (-) m/z 59.00 100.00% 59

5000 ,.** A 45 73 86 । 9.60 9.80 10.00 10.20

m/z-> 0- ............. 20 30 nu...... 40 50 I |।60.....1)1 70 80 90 100 110 120 m/z 45.00 10.04% Abundance #15890: Hexanamide $$ n-Caproamide $$ n-Hexanamide $$ Capr... 59

5000 9.60 9.80 10,00 10.20 44 72 m/z 43.00 9.97% 27 86 ____ L | 115 0- ' I r. | " I1' 1 ' i 1 • 1 I 1 1 1 ' r ■ ' i ' ■ 1 ' i ■ ' ■ ■ i ■ ' ■ ■ i ' ■ ■ ■ i ■ ' n/z-> 20 30 40 50 60 7080 90 100 110 120 Abundance #3753:3-Butenoic acid $$ .beta.-Butenoic acid $$ Acetic a... 39 — 9.60 9.80 10,00 10.20 5000 m/ z 85.80 9.27% 45 58 86 68 0-IPPT H= Anbggdnqlut 1 ■ i ■ 1 i ■ ■ 1 ' i ■ ■ 1 ■ i ‘ ■ i ■ ■ z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance ;#3751:3-Butenoic acid (CAS) $$ Vinylacetic acid $$ .beta.... 39 9.60 9.80 10.00 10.20 m/z 42.00 9.09% 5000 45 58 86 68

m/z-> 0 1 । 1 ■ 1 ■ । 20 30 ' 40 1 1 i 1 50 jan 11 60 70 ......... 80 90 100 110 120 9,60 9.80 10.00 10.20

)3248.D HP022102.M Mon Mar 04 12:33:28 2002 Page 9

NYC-WTC_000006158