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GCMS results for sample AE00737, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051930–000051947

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051942
OCR text

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00737.D Vial: 5 Acq On : 16 Jan 2002 6:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1-butoxy- (CAS)... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.26 ug/L 99196 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-butoxy- (CAS) $$ 1... 132 C7H1602 005131-66-8 72 2 Formic acid, 1-methylpropyl este... 102 C5H10O2 000589-40-2 36 3 Morpholine 87 C4H9NO 000110-91-8 35 4 2-Butanol, 3,3-dimethyl- (CAS) $... 102 C6H140 000464-07-3 33 Abundance Scan 425 (8.226 min): 00737.D (-) m/z 45.10 100.00% 45 57

87 5000

i > • • ■ । ■ .................. A,, 39 , 7.80 8.00 8.20 8.40 8.60

n/z-> 0- .... 10 20 . 30 Ilil 40 50 ■ i ■ 70 ' 80 I — 60 100 • I ' ' ' ' I • i ■ • • • i 110 m/z 57.10 92.30% Abundance #28054:2-Propanol, 1-butoxy- (CAS) $$ 1-N-BUTOXY-2-PROPAN... 45 57

5000 Pmyemmm 7.80 8.00 8.20 8.40 8.60 31 87 m/z 87.10 50.29% 75 । ''i ■ 1 1 ■ i ■ ■ ' ■ i 0 71 i ' ' ' ' i ' ' ■ ■ i ' ' ' ■ i ' ■ 1 ' i 1 ■ i' ’ ■ ■ i ■ ’■ ■ • i

/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9300: Formic acid, 1-methylpropyl ester (CAS) $$ sec-Buty... 45 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.10 46.19% 56 31 73 ll 87 102■ ■ < i O' 1 I ' 1 1 1 I ■ i ' 1 i 1 । >■ I T TPTr ("I i ■ । ■ ■ ■ ■ । ■ i < 80 90 100 110 n/z-> Abundance 10 20 30 40 50 60 70 #4373: Morpholine A J 29 57 7.80 8.00 8.20 8.40 8.60 87 m/z 56.10 33.51% 5000

15 42 - 0—T i____ ------- ' i ' ■ ■ ■ i ' ■ ■ ■ i ' ' -1 • ■ ■ i m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

00737.D SCAN508.M Thu Jan 17 08:17:40 2002 Page 9

NYC-WTC_000051942

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NYC-WTC_000051942Source: NYC Law Department, mirrored locally

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