GCMS analysis results for sample AE00844, Feb 26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 7 2-Propanol, l,l'-oxybis- (C... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

9.56 0.07 ug/L 26690 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 9 4 2,3-Epoxy-3-methyl-6-methoxyheptane 158 C9H18O2 088083-53-8 9 Abundance Scan 542 (9.562 min): 00844.D (-) m/z 59.10 100.00% 59

5000 45 73 103 -Innnmm "I "TI" 86 9.20 9.40 9.60 9.80 OTT m/z 45.10 43.21% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29204: 2-Propanol, 1,1'-oxybis- (CAS) $$ Dipropylene glyc... 59

31 5000 45 103 9.20 9.40 9.60 9.80 m/z 41.10 29.16%

0- — n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29205: 2-Propanol, 1,1'-oxybis- (CAS) $$ Dipropylene glyc... 59 31 5000 45 m/z 103.10 28.20% 103

O' | 1 1 'ip TTT ' i ' ■ ' ■ i ' ■ ' ■ i ' ' ' ■ i 1 • ■ 1 i ■ ' ■ ' i ■ 1 ■ ' i ' ' ‘ ' i 1 ' ' ' i ■ 1 ' ' i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #61826: 2-Butanol, 3,3'-oxybis- - । ■ > t ■ । ■ ■ ■ • । ■ 1 i i 1 59 9 20 9.40 9.60 9.80 m/z 73.10 27.45%

5000 31 45 103

0 7 1— 4 11 ■ ■ ■ ■ ।1111111111111 11 1 l > > p । r 134 , Irrr i ITTT // AA— m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

00844.D HP020702.M Thu Feb 21 09:58:17 2002 Page 9

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