GCMS results for sample AE00560, Jan 17 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00560.D Vial: 4 Acq On : 15 Jan 2002 4:00 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 2-Propanol, l,l'-oxybis- (C... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 9.64 0.11 ug/L 35027 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 40 2 Z-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 3 1-Propanol, 2-(2-hydroxypropoxy)... 134 C6H14O3 000106-62-7 9 4 BIS(1-METHYL-2-HYDROXYETHYL)ETHER 134 C6H1403 000000-00-0 9 Abundance Scan 549 (9.642 min): 00560.D (-) m/z 59.10 100.00% 59

5000

0 i • *' ■ i1' " r ■ ■ ■ i 45

— ■ ■ । > 11 > ■ ■ । ■ 73 103

m/z 9.40 M • ■

45.05 9.60 l ■ ■ ■ ■

9.80 I ■

10.00 38.14% ' i ■ ■ ■ ■ i' ■ ■ ■ i" ■' i " ■ ■ i ■ ■ ■ ■ i ■ ■ ■ r '1 • r ■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #29204:2-Propanol, 1,1'-oxybis- (CAS) $$ Dipropylene glyc... 59

31 5000 45 103 9.40 9.60 9.80 1000 m/z 41.10 35.98%

n/z-> 0 T‘ .... U..... iiL -PH i" " i’’ " i""r■"r ■ ■ ■ r■ ‘ ■ l■■ ■■ i "r' 11 " '-' T'1 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #29238: Z-Dipropylene glycol $$ 2-hydroxyethyl ether 50 31 9.40 9 60 9 80 10.00 5000 m/z 103.10 35.77% 45 103

0 i""i""i MH+l H MM n/z—> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #29195:1-Propanol, 2-(2-hydroxypropoxy)- $$ 2-(2-Hydroxyp... 59 9.40 9.60 1 TB 9.80 10.00 m/z 73.00 33.45%

5000 31 45 103

0 la TPTTH Pmmmmmmupt i" " i .........." 75 89 M.,M... n/z-> :20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 9.40 9.60 9.80 10.00

00560.D SCAN508.M Wed Jan 16 08:14:10 2002 Page 7

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