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GCMS results for sample AE00697, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051860–000051876

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00697.D Vial: 3 , Acq On : 16 Jan 2002 12:31 pm Operator: Sample : 508scan Inst : Instrumen Misc : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 9.55 0.12 ug/L 40163 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H1603 020324-32-7 43 2 BIS(1-METHYL-2 -HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 9 3 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 4 2-Propanol, 1-(2-ethoxypropoxy) - 162 C8H18O3 010143-32-5 9 Abundance Scan 541 (9.550 min): 00697.D (-) m/z 59.10 100.00% 50

n/z-> 5000

0-TPT 20 30 l.. .. 40 45

50 60 80 70 73

90 100 110 120 130 103

140 9.20 m/z 103.10 9.40 AN 9.60 9.80 43.94% Abundance #43943:2-Propanol, 1-(2-methoxy-1 -methylethoxy)- $$ Dipro... 50

5000 45 103 9.20 9.40 9.60 9.80 73 31 m/z 45.10. 39.89% O—TT ' 1 o .. | I Ji i | । i । I. ....... t ......................।.................... 130........ m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #29208: BIS(1-METHYL-2-HYDROXYETHYL)ETHER 50 1 ' i 1 1 1 1 r1 1 1 1 i ■ ■ ■ ■ i ' ■ ■ 1 i ■ 9.20 9,40 9.60 9.80 5000 31 m/z 41.10 26.67% 45 103

O ' ।11''' r 1 —4 1 ' i ' ■ I' ■ ■ ■ i ■ ' ■ ■ i ■ ■ ■ ■ I 1 1 1 1 I 1 134 1 " I " " I " ' ' I ' 1 ' ' I ' /z-> 20 30 40 50 (60 70 80 90 100 110 1 20 130 140 Abundance #29239: E-Dipropylene glycol $$ 2-hydroxyethyl ether 31 50 9.20 9.40 9.60 9.80 m/z 73.00 21.80%

5000 45 103 39. O—P s , 11 . ।. ...... ........ ........................ 1 1 1 i 11 1 1 i ■ 1 ■ ■ । ' i' A NA m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

00697.D SCAN508.M Thu Jan 17 08:16:55 2002 Page 7

NYC-WTC_000051870

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NYC-WTC_000051870Source: NYC Law Department, mirrored locally

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