GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051860–000051876Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
1 ~upOul RSDUL L
Data File : C:\MSDCHEM\1\5973N\02JAN16\00697.D Vial: 3 Acq On : 16 Jan 2002 12:31 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Propanol, 1-butoxy- (CAS)... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 8.23 0.25 ug/L 80592 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1-butoxy- (CAS) $$ 1... 132 C7H16O2 005131-66-8 74 2 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 38 3 2-Propanol, 1-butoxy- (CAS) $$ 1... 132 C7H1602 005131-66-8 38 4 Pinacolyl alcohol__________________ 102 C6H140 000464-07-3 36 Abundance Scan 425 (8.226 min): 00697.D (-) m/ Z 45.10 100.00% 45 57
5000 87
—A 39 I I7,5 7.80 8.00 8.20 8.40 8.60 Oh TTTTTTPTTTTT ' u ""i ■■1 ■ i" M " "i"" i m/z 57.10 91.49% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #28054:2-Propanol, 1-butoxy- (CAS) $$ 1-N-BUTOXY-2-PROPAN... 45 57
5000 i ■ ■ ■ ' i ■ 1 7.80 8.00 8.20 8.40 8.60 31 87 m/ z 87.10 46.40% 75 0 1 ‘1' i ■ ■r' i ■"11'1 ■ ■ ।1 TIT H 'i'" ri' HTT > I j+ri 1111 > 111 > > < 111 ■ 11111H । i" " r"' i" " i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #4372: Morpholine (CAS) $$ BASF 238 $$ Diethylene oximide ... 29 57 । 1 1 ■ 1 । • ■ ' ■ । ' ' ■ । 1 ■ ' ■ । 1 ■ ■ 7.80 8.00 8.20 8.40 8.60 5000 rn/z 41.10 37.34% 87
15 42 Oh '11 T >H|IIII|II!I|HI1| t> ।।■ 11 >> >■ । >•■11 ■ > • ■ । m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #28051: 2-Propanol, 1-butoxy- (CAS) $$ 1-N-BUTOXY-2-PROPAN... 45 57 7.80 8.00 8.20 8.40 8.60 m/z 56.10 33.54% 5000 27 87 15 75 Oh mm —m 33 ‘ I Pgun 101 mHHemTTTTTTTTTTTTT ■ 'i" "i" " i' m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.80 8.00 8.20 8.40 8.60
0697.D SCAN508.M Thu Jan 17 08:16:55 2002 Page 6
NYC-WTC_000051869
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NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051948
Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051697
Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder