GCMS results for sample AE00697, Jan 29 2002

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN16\00697.D Vial: 3 Acq On : 16 Jan 2002 12:31 pm Operator: Sample : 508scan Inst : Instrument Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Propanol, 1,1'-oxybis- (C... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.64 0.13 ug/L 43232 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1,1‘-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 50 2 2-Propanol, 1,1‘-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 9 4 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 Abundance Scan 549 (9.642 min): 00697.D (-) m/z 59.10 100.00% 59

5000 45 73 103

9.40 9.60 9.80 10.00 1 ' I. . । । । ।। । .1। । । । . O' I 1 1 1 1 1 1 m/z 45.10 46.45% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29204: 2-Propanol, 1,1*-oxybis- (CAS) $$ Dipropylene glyc... 50

31 5000 45 Tr 103 9.40 9.60 9.80 10.00 m/z 103.05 30.16% 0-TT A1..... 1"....... hl........ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29205: 2-Propanol, 1,1 '-oxybis- (CAS) $$ bipropylene glyc... 59

31 9.40 9.60 9.80 10.00 5000 45 m/z 73.10 26.07% 103

niz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #61826: 2-Butanol, 3,3‘-oxybis- 59 ..... MM,M, 9,40 9.60 9.80 10.00 m/z 41.10 24.67%

5000 31 45 103

O-T —4 TTPPTT ■ i ' 1 ■ ■ i 1 ■ ■ 1 i ■ ' 1 1 i 1 1 ' ■ i ' ' ' ' i ■ ' 1 1 I 134 ■ 1 ' ' i ' m/z-> 20 30 40 50 I60 70 80 90 100 110 120 130 140 9.40 9 60 9.80 10.00

00697.D SCAN508.M Thu Jan 17 08:16:55 2002 Page 8

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