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GCMS results for sample AE00560, Jan 17 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051740–000051754

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051749
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00560.D Vial: 4 Acq On : 15 Jan 2002 4:00 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 4 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 9.55 0.14 ug/L 44039 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 64 2 BIS(1-METHYL-2 -HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 9 3 2-Propanol, 1-(2-ethoxypropoxy)- 162 C8H18O3 010143-32-5 9 4 MIXTURE OF: 5-METHOXY-3 -PENTEN-2. . 116 C6H12O2 072649-04-8 9 Abundance Scan 541 (9.550 min): 00560.D (-) m/z 59.10 100.00% 59

5000 45 73 84 103

9.20 9.40 M ■ ■ l ■ ' ' • I 9.60 9.80 0-T mmppos)....... - m/z 45.10 43.28% •n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #43943:2-Propanol, 1-(2-methoxy-1 -methylethoxy)- $$ Dipro... 59

5000 45 73 103 9.20 9 40 9.60 A9.80 T

31 m/z 103.10 41.99% ,.................... .................................... 130.......... 01 ... . ■ ■ i । ' 1 —IPH 11 T)/Z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29208: BIS(1 -METHYL-2-HYDROXYETHYL)ETHER 59 1 Tl TT 9.20 9.40 9.60 9.80 5000 31 m/z 73.10 25.05% 45 103

O—TTTT —4 T-r-i-r 111 ■ i ■ ■ ■ ■ i ■ ■ ■ • । 134 > i • i > • i ■ • ■ > । > • • > । ■ ■ ■ ■ । > /z- > Abundance 20 30 40 50 60 70 80 90 100 110 #61828: 2-Propanol, 1 -(2-ethoxypropoxy)- 59 120 130 140

9.20 9.40 ANAA 9.60 9.80 m/ z 41.10 20.49% 45 5000 31 73 103 87 1....... 118................... 0—1P P-P ■ i ' • ■ ''i ■ Wz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

00560.D SCAN508.M Wed Jan 16 08:14:09 2002 Page 6

NYC-WTC_000051749

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NYC-WTC_000051749Source: NYC Law Department, mirrored locally

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