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GCMS results for sample AE00700, Feb 13 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00700 showing surrogate recovery and unknown compounds detected on February 13, 2002.

NYC-WTC_000051806–000051824

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051818
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB01\00700.D Vial: 7 ‘ Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1 - (2-methoxypro . . . Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 9.86 0.16 ug/L 60656 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxypropoxy) . . . 148 C7H16O3 013429-07-7 83 2 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 9 3 1-Propene/ 2-fluoro- (CAS) $$ 2-... 60 C3H5F 001184-60-7 9 4 3-Heptanal (CAS) $$ 3-Hydroxyhep... 116 C7H160 000589-82-2 9 Abundance Scan 568 (9.859 min): 00700.D (-) m/z 59.10 100.00% 59 ___

5000

73 104 9.60 9.80 10.00 10.20 Of • I • • • • I • ITT - m/z 45.10 15.08% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 9.80 10.00 10.20 m/z 43.10 9.21% 31 45 ----- 73 104 130 0 ■ i ■ ' I................ . ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... 31 59 9.60 9.80 10.00 10.20 5000 m/z; 73.10 8.27%

45 104 ..I... .. I m/z-> Abundance 0 ■ i ’ > 20 30 40 50 60 70 80 90 100 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I ' 1 110 #762:1-Propene, 2-fluoro- (CAS) $$ 2-Fluoropropene $$ Pro... 59 120 130 A,/. 960 9.80 10.00 10.20 m/z 41.10 7.01% 39 5000

33 45

-nlz-> 0 ........ 20 30 al’40l........ 50 60 ‘ 70 80 90 100 110 120 130 9.60 9.80 A 10.00 10.20

00700.D SCAN508.M Mon Feb 04 08:40:51 2002 Page 9

NYC-WTC_000051818

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NYC-WTC_000051818Source: NYC Law Department, mirrored locally

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