GCMS results for sample AE00737, Jan 29 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00737.D Vial: 5 . Acq On : 16 Jan 2002 6:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 PROPYLENE GLYCOL TRIMER 3 Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.16 ug/L 61964 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 PROPYLENE GLYCOL TRIMER 3 174 C9H18O3 000000-00-0 74 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 64 3 Butane, 1-ethoxy- (CAS) $$ Ethyl... 102 C6H140 000628-81-9 9 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 Abundance Scan 567 (9.847 min): 00737.D (-) m/z 59.10 100.00% 59

5000

0 45 ..... mJ...... । 73 04 |.......... I................ 103 lp rn/ Z N 9.60 9.80 45.10 1 11 । । । f । । । 10.00 10.20 15.06% /z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78534: PROPYLENE GLYCOL TRIMER 3 59

5000 41 103 9.60 9.80 10.00 10.20 m/z 43.10 10.49% 1 0— 1 1 1 । 1 > , । , ' mh..... -i'. 73 87 117 130 n/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOLTRIMER 1 59 11, 9.60 9.80 1000 10.20 5000 41 m/ Z 42.10 8.05% 103

73 — ... m,... 11, o7 117 130 oV ... .. .... . 1 ■ ■ i ■ ■ ■ ' i ■ ■ ■ ' i ' ■ n/z-> 30 40 50 60 70 80 90 100110 120 130 Abundance 1,4,4/, #9713: Butane, 1-ethoxy- (CAS) $$ Ethyl butyl ether $$ Eth... 59 yC.......... 9.60 9.80 10.00 10.20 m/z 41.10 7.33% A 5000 41 73 87 102 m/z-> 0— 30 40 — — — — 50 4 ---****—*** 60 70 80 90 100 110 120 130 9.60 9.80 IT ■ • । ■ 1 10.00 10.20

10737.D SCAN508.M Thu Jan 17 08:17:40 2002 Page 10

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