GCMS surrogate recovery results for sample AE00281, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\281.D vial: 6 Acq On : 9 Jan 2002 10:21 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1-(2-methoxypro... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 9.85 0.23 ug/L 128025 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 74 3 PROPYLENE GLYCOL TRIMER 3 174 C9H18O3 000000-00-0 43 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 40 Abundance Scan 567 (9.847 min): 281 .D (-) m/z 59.10 100.00% 59

5000

45 — 73 104 M 9.60 9.80 --P44- 10.00 10.20

m/z-> 0- 30 40 50 60 111 70 80 84.90). 100 ,l....... 110 120 130 m/z 45.10 11.92% Abundance #43942: 2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 AA ‘I iif —4 9.80 10.00 10.20 m/z 73.00 9.19% 31 45 73 104 0- 1 1 ■ r ........................ 171............... 130 1 I ' ■ ' ■ i ' ' ■ ■ i ■ ■ ■ ■ i ■ 1 ■ ■ 1 ' ■ ' 1 1 ' ' ■ ■ i ' ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOL TRIMER 1 59 —

9,60 9.80 10.00 10.20 5000 41 m/z 58.10 8.26% 103

- 73 0 —44 TI—87mBTTT’T 117 130

..i. I TITT 1 ■ 1 I > 1 <■■ । > ■ * - । । ■ n/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #78534: PROPYLENE GLYCOL TRIMER 3 59 960 9.80 IQ.'OO 10.20) m/ z 42.10 8.12%

5000 41 103

73 87 ................ 117 130 0 ■ • 1 • > • • । l ■ • • । ■ All r ■ s ' ■ i ' > i ■ , , A ( 1 1 | '■ 1 \ I | I I I ! | |" I

/z-> 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

281.D SCAN508.M Thu Jan 10 11:52:01 2002 Page 11

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