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GCMS surrogate recovery results for sample AE00281, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.

NYC-WTC_000050912–000050931

Folder label: “GCMS X 1/7/02 A 1/9/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\5973N\02JAN09\281.D Vial: 6 Acq On 9 Jan 2002 10:21 pm Operator: Sample 508 scan ext 1/7 Inst Instrumen Mise January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 8 2-Propanone, 1,1,1-trichlor... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.00 0.52 ug/L 288549 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 64 2 2-Propanone, 1,1,1-trichloro- $$... 160 C3H3C13O 000918-00-3 50 3 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 42 4 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 42 Abundance Scan 230 (6 000 min): 281 D (-) m/z 43.10 100.00% 43

5000

0-1**1w—TTTHt +49-61 — 70 ..80 36 97 |, 117 125 5.60 5.80 m/z 124.90 6.00 6.20 6.40 9.37% /z-> 10 20 30 40 50 60 90 100 110 120 130 Abundance #59078:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43

— 5000 ' I 1 r ‘"I ' < l ■ ■ ■ ■ । ■ 5.60 5.80 6.00 6.20 6.40 m/z 97.00 6.58% 61 82 97 117 125 o1 ■11 ■1 ■11 ■ ■ ■' । ■35 49 11111111111 , , 1 ■ । ■ । ! I l'i , । । 1, I m mgmli । , n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59081: 2-Propanone, 1,1,1-trichloro-$$ alpha ,.alpha...... 43 5 60 5.80 6.00 6.20 6.40 5000 m/z 47.00 5.94%

15 A 35 ,49 85 97 117 125 o1 •11 ■ ■'1 FTu '1 r"''1111 TH-nB—TTTT—PTTPTTPTTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59082:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... A A 43 5.60 5.80 6.00 6.20 6.40 m/z 127.00 5.78% 5000

15 27 f 49 63 110 117 127 0 TTPPTTTTPTTT /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

181. D SCAN508.M Thu Jan 10 11:52:01 2002 Page 10

NYC-WTC_000050926

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NYC-WTC_000050926Source: NYC Law Department, mirrored locally

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