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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01141.D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L

Peak Number 4 2-Propanone, 1,1,1-trichlor... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.00 0.31 ug/L 127618 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- (C. . . 160 C3H3C130 000918-00-3 83 2 2-Propanone, 1,1,1-trichloro- $$. . . 160 C3H3C130 000918-00-3 78 3 2-Propanone, 1,1,1-trichloro- (C. . . 160 C3H3C130 000918-00-3 53 4 2 -Propanone, 1,1,1-trichloro- (C. . . 160 C3H3C130 000918-00-3 45 Abundance Scan 233 (6.004 min): 01141.0 (-) m/ z 43.10 100.00% 43

5000

49 61 83 9/ 117 125 5.60 5.80 6.00 6.20 6.40 01 1I*I**I*| I1 1 I ' ■ ] I I I I - P1 1 1^1 I I I - I I I [ I11 J.1. _______________ _ 1 J 111 I , ’ll I I I I ■ > I I I I I I I I I > I I . > I I ′ m/z 124.90 7.20% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59078:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43

5000 5.60 5.80 6.00 6.20 6.40 m/z 126.90 6.64% 49 35 - 61 82 97 117 o1 111111* m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59081: 2-Propanone, 1,1,1 -trichloro- $$ .alpha.,.alpha.... 4)3 ' I ' ' ‘ ' 1 1 ' 5.60 5.80 6.00 6.20 6.40 5000 m/z 82.90 6.35%

15 35 85 97 117 125 01 ..... mH...... 111.49, ■ 1 i ' ' ■ 1 i ' ■ ' 1 i 1 1 ' ' i ■ ' ''''i > ■ ■ ■ । - '"'‘i ' te’s । ' ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59082:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 4)3 5.60 5.80 6.00 6.20 6.40 m/z 47.00 6.28%

5000

15 27 49 63 85 97 110 117 127 0 > ■ i ■ ■I ■ > i ■ ■ ■ ■ । । । "'I.. ’ i 1 1 । 1 1 1 1 i ■ ■ ■ ■ i ■ 1 ■ ■ i ' ■ ■ ■ I ' 1 i ■ 1,1 i 1 ' ■ i ■ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

01141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 6

NYC-WTC_000003552

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NYC-WTC_000003552Source: NYC Law Department, mirrored locally

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