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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01141.D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak.Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.33 ug/L 138149 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3' -EN-YL) PROPANOL $$... 174 C8H14O4 015745-87-6 42 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 42 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 N,N-DIMETHYL-2-BUTOXYISOPROPYLAMINE 159 C9H21NO 000000-00-0 9 Abundance Scan 228 (5.947 min): 01141 .D (-) m/z 73.10 100.00% 7)3

5000 43 ■ ■ । ■ 1 1 ■ । ■ ■ 1■ । ■ na । . 5.60 5.80 6.00 6.20 ............ IL 55 0- • ['111 11 1' »I»• ‘1 I ! l I >' ■ ''''i , 87 103 11 11" m/z 43.10 23.80% niz- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ■ ■ l 1 ' I FITPIIII 5.60 5.80 6.00 6.20 43 m/z 45.00 10.14% 27 , 87 113 55174 , i 0- Tp TIWTTTTTTT TTu—I———uuuuIIORTT /z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.75% 43 27 55 . 1 , 87 113 174 0-TTTTTTTTT ' i ‘ ' i1" 'T' ' " i " 1' i " " i ■' " i " i " " i “ 11111" i " " i1 " ' i1' " i' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 1 l ' ' ' ' I ' 1 1 1 l ' 30 5.60 5.80 6.00 6.20 73 m/z 71.00 6.71%

5000 44 58

15 0 "111 I"11 TI TTTTTITTORmuumTg /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 5

NYC-WTC_000003551

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NYC-WTC_000003551Source: NYC Law Department, mirrored locally

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GCMS analysis results, Feb 27 2002 · Box DEP Box 12

NYC-WTC_000003463

Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

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