GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 3-(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.28 ug/L 1574670 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 Abundance Scan 220 (5.885 min): 00700.0 (-) m/z 73.10 100.00% 70

5000

43 . । , , ‘III , 1 ■ i 1 1 ■ ■ 5.60 5.80 6.00 6.20 , 87 103

m/z-> 01■ ’ r ' " i' " 11' 1 0,11155%... J " " I ’ I ' 1 " I t’rrii I । > I | । I I I | I I! I | । I I ! | I

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/ z 43.10 23.78% Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70

5000 *‘‘11117 "T I I I | Py 5.60 5.80 6.00 6.20 43 m/z 45.10 8.76% 27 55 87 o1'11" " i' " ' i' — .| . 113 174 T‘ "" i "1 ■ i1 ■" i1'111' i I " ‘11 n/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.72% 43 27 55 , 87 113 174 0"i""i" TTTTH ' i " " r ■ ■ • i • "" i"1' i "11111 Tliri 11111111111111111111111 i' r "' [ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... IP r'r i 1 11 1 30 5.60 5.80 6 00 6.20 73 m/z 71.10 6.54%

5000 .................... _ 44 58

15 0 -P ..... W..... ।" "i '1"i" ■ ■ i ‘ "■ i""i■" ■ i" ■ ■ i■" ■ ।"" । ■ ■■11■1" । ■11 ■ i■ n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

30700.D SCAN508.M Thu Jan 17 08:17:09 2002 Page 3

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