GCMS analysis results for sample AE00842, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.

NYC-WTC_000052251–000052270

Folder label: “GCMS X 1/11/02 A 2/7/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00842.D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.92 0.42 ug/L 172569 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 40 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 40 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-(6-heptynyl) -168 C10H16O2 025595-82-8 9 Abundance Scan 223 (5.920 min): 00842.D (-) m/ z 73.10 100.00% 73

5000

m/z-> 0 +1 I' u ' l' " ’ I 1 87 43 103 55 T’TTT 151 " • • | • ' >'■ ] I । । | 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I ' | । । | । I • | I * ■ I | । | ' • ' ' | TT m/z 5.60 5.80 43.10 L6.00 6.20 22.97% Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 78

5000 .. N_. I . . | , I I I | I |'| , | 5.60 5.80 6.00 ri ri rr 6.20 43 m/z 45.10 10.30% 27 .|55 113 87 174 OT) I’ts i' " ■ i ' MT ‘‘‘ ' I ' I.. i ''1' r i ■ ■'' i' •'' r " ' i i m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7)3 TT 5.60 5.80 6.00 6.20 5000 m/z 41.10 10.09% 43 27 87 0- i ■'" i' " ' i + 55 T+ MT 113 , 1 r 174 r "' r i " '' i'1 ■' i ■'1' r ■' ■ i'' " r " ' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 3b 5.60 5.80 6.00 6.20 73 m/z 71.00 7.43% 5000 44 58 15 0 _j___ i ■■ ■ • । — 'l ' 1 1 ' T *muuwnmwnmw*oumuunu*nn)nnmT TT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00842.D HP020702.M Thu Feb 21 09:58:09 2002 Page 7

NYC-WTC_000052261

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NYC-WTC_000052261Source: NYC Law Department, mirrored locally

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