GCMS analysis results for sample AE01142, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE01142 conducted on February 27, 2002.

NYC-WTC_000003523–000003542

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01142.D Vial: 8 Acq On : 25 Feb 2002 5:01 pm Operator: • ■ Sample : 508 scan Inst : Instrumen Mise 2002 : February 25, Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.94 0.32 ug/L 137872 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 38 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 38 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-pentadecyl- $$ ... 284 C18H36O2 004360-57-0 9 Abundance Scan 227 (5.936 min): 01142.D (-) m/ z 73.10 100.00% 73

5000 43 , । 55 |.. 87.. 103...................... 5.60 5.80 6.00 6.20 0- । i 11 i 11 । । , r T . /‘ Il II rp. 141′11 t r 1 । Ij I . m/z 43.10 22.32% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000- 1 ■ i ■ ' ' ' i ' 1 1 ‘ i ■ ■ ' ■ i ■ ■ ' ' i 5.60 5.80 6.00 6.20 43 m/z 45.10 8.83% 27 55 87 113 174 0- TTTTT ' i ‘1 " i " ' 'T' ■ i — 11 " i " " i " ' ■ r ■ " i ■ “ ' ir " ' i1' " i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 1111‘‘11‘I+141I‘ ‘IY 5.60 5.80 6.00 6.20 5000 m/z 41.10 7.52% 43 27 55 87 113 0- '11 ■1" i ■ i' TTH4 ■ i " " i'11 ‘, ii 1 - ■ i ■" ■ ।। ‘1111" ।।। 174 ।1 '"I1"1!' M m/z- > Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 1 ■ i ' ■ ■ ' i ■ 5.60 5.80 LAA_ 6.00 6.20 73 m/z 71.10 5.16% 5000 44 58

15 m/z-> 0- -HH ’l " ‘ ′ i < । । । I i j । । > । । > । । । । । " । । । । । < । i > । I j i | । i j । > < । । । । >> । .> । i । ।

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31142.D HP022102.M Tue Feb 26 08:30:34 2002 Page 7

NYC-WTC_000003533

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NYC-WTC_000003533Source: NYC Law Department, mirrored locally

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GCMS analysis results, Feb 27 2002 · Box DEP Box 12

NYC-WTC_000003463

Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

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