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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01141.D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: . • Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.37 ug/L 227463 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 80 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H40O5Si4 037148-65-5 38 4 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 36 Abundance Scan 812 (12.540 min): 01141. D (-) m/z 73.00 100.00% 73 A 5000 267 355

12.20 12.40 12.60 12.80 45 133154 193 0+ ' I.] ’I 237—1— i ■ 323 ■ m/z 266.90 40.34% miz-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 ,................... 5000- 12.20 12.40 12.60 12.80 m/z 355.00 37.43%

Ot ■ i 1 11 “I" 207 250 -2- 400 300 450 350 m/z-> 50 100 150 200 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ............... 1 ' 1 i ■ ■ ' ■ i ' ■ ' ■ ' ' i ' ■ ' ■ i 12.20 12.40 12.60 12.80 5000 267 m/z 356.00 13.30% 355 45 I I , O+ 'I ‘ ' . 193 23.4.4 —323—4 m/z-> 50 100 150 200 250 300 350 400 450 - Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 12.20 12.40 12.60 12.80 m/ z 268.00 11.03%

5000 355

147 0 I ,L 193 267 295 t 429 457 -TT ...................... 1 i ■ ■ 1 ■ i ■ ■ ' ' i ■ ■ i • ■ ' ■ i ' ' miz-> 50 100 150 200 250 300 350 400 450 12.20 12.40 12.60 12.80

01141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 7

NYC-WTC_000003553

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NYC-WTC_000003553Source: NYC Law Department, mirrored locally

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