GCMS analysis results for sample AE01141, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01141 .D vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.06 ug/L 39172 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 78 2 4H-Pyran-4-one, 2-ethyl-3-hydrox... 140 C7H803 004940-11-8 56 3 Pyridine, 4-nitro-, 1-oxide (CAS... 140 C5H4N2O3 001124-33-0 50 4 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 39 Abundance Scan 886 (13.375 min): 01141.D (-) m/z 140.00 100.00% 140

5000

70 84 94 108 13.00 13.20 13.40 13.60 13.80 44 54 Ot 111—1 d./ | ‘II m/z 94.00 13.11% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 13.00 13.20 13.40 13.60 13.80 54 68 m/z 69.90 12.79% 80 95 10S 121 n/z-> ot 30 40 1 ' i ' 60 50 70 ■ ■ ।1 ■ 80 90 100 110 120 130 I... I..... I,,.... 140I 1dr

Abundance #35346:4H-Pyran-4-one, 2-ethyl-3-hydroxy- (CAS) $$ Ethyl... 140 ' i 1 1 ' 1 i 0.......... 13.00 13.20 13.40 13.60 13.80 5000 97 m/z 141.00 9.88% 71 125 53 84 111 - Of -P 1 1 ' 1 1 1 1 . tn-p-r TIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35067: Pyridine, 4-nitro-, 1-oxide (CAS) $$ p-Nitropyridi... 140 13.00 13.20 13.40 13.60 13.80 m/ Z 66.00 9.87%

5000 39 110 51 45 63 124 84 94 —L TdI 0 ------- ----- m/z-> 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

01141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 8

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