GCMS analysis results for sample AE03245, March 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 • Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Pyrimidinetetramine- $$ Pyr... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 27203 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 64 2 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 50 3 3H-Pyrazol-3-one, 2,4-dihydro-2,... 140 C7H12N20 003201-25-0 42 4 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N4O 000000-00-0 40 Abundance Scan 886 (13.376 min): 03245.D (-) m/z 140.00 100.00% 140

5000 W...... . 49 70 86 86 106 । 13.00 13.20 13.40 13.60 13.80

n/z-> 0- 1 ■ । ■ ■ ■ ' । 1 1 1 ■ । 40 50 60 70 ■ 4 80 90 100 110 120 130 140 1di rn/z 70.00 12.87% Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

5000 1 i 1 ■ ' ' । 1 13.00 13.20 13.40 13.60 13.80 44 71 123 m/z 140.90 12.43% | 86 96 112 0- --------- । | m/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 1T -n-|-r-r-|-|-|-r

82 13.00 13.20 13.40 13.60 13.80 5000 m/ z 68.20 11.61%

54 68 96 | 111 o1 T-' | 1 - 1 11.1 +T 1IT m/z-> 40 50 60 70 80 90 100 110 120 130 140 - Abundance #35412: 3H-Pyrazol-3-one, 2,4-dihydro-2,4,4,5-tetramethyl-... 1-0 13.00 13.20 13.40 13.60 13.80 41 69 m/z 108.10 11.57%

5000 97

125

m/z-> 0 ■ ' 1 1 40 53 - > r >1 ■ 1 - j > । ■ I 50 60 70 —P , 82

80 90 100 1 i 1 ' 1 1 i ' 1 1 1 1 1 1 1 1 1 1T 110 120 130 11 TII 140 13.00 13.20 13.40 13.60 13.80

)3245.D HP022102.M Mon Mar 04 12:33:07 2002 Page 14

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