GCMS analysis results for sample AE03250, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03250 conducted on March 15, 2002.

NYC-WTC_000006186–000006205

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 . Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************* * * * ********* * * * * * * * * ****************** Peak Number 11 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.06 ug/L 39085 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 56 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 56 3 Pyridine, 4-nitro-, 1-oxide (CAS... 140 C5H4N2O3 001124-33-0 50 4 Cyclobuta [de] naphthalene 140 C11H8 024973-91-9 9 Abundance Scan 886 (13.376 min): 03250.D (-) m/z 140.00 100.00% 140

5000

............ ........................... 70 13.00 13.20 13.40 13.60 13.80 43 49 n/z-> Of ' I ' ' ' ' I ' 1 ' ' I ' 1 ' ' I ,-r । । | । 30 40 50 60 70 80 90 100 110 120 130 —140L "II m/z 70.00 14.86% Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140

42 ... / 5000 1 1 i 1 ■ ' 1 i ■

54 13.00 13.20 13.40 13.60 13.80 68 m/ Z 141.00 11.90% 80 95 108 121 01 ■ ' i ' 1 ., T I. —L ‘II m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

13.00 13.20 13.40 13.60 13.80 5000 m/ Z 94.00 10.88% 44 71 123 86 96 112

miz-> Of ........ 11. 30 40 50 I 1 1 1 1 I . 1 1 1 | . 1 । . I 1 60 70 80 I 90 100 110 120 130 140 1IT

Abundance #35067: Pyridine, 4-nitro-, 1-oxide (CAS) $$ p-Nitropyridi... 1 | I 1 1 | 1 1 1 O| ' 1 ! I | ! . . . | . to 13.00 13.20 13.40 13.60 13.80 m/z 96.00 10.87%

5000 39 110 51 45 63 124 84 94

m/z-> 0 —P 30 ■ t • I • ‘ l > ■ ■ 1 I I I 1 1 i1 1 1 1 i 1 । 1 1 i1 40 50 60 70 80 1v’ 1 1 — —L 90 100 110 120 130 140 Tit 13.00 13.20 13.40 13.60 13.80

I3250.D HP022102.M Mon Mar 04 12:33:42 2002 Page 13

NYC-WTC_000006202

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