GCMS analysis results for sample AE03252, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03252.D Vial: 7 . Acq On : 1 Mar 2002 8:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 6 2-Methoxy-3-hydrazinyl-pyra ... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.05 ug/L 31599 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 64 2 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 64 3 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 64 4 9-Oxabicyclo[3.3.1]nonan-2-one 140 C8H12O2 019740-79-5 9 Abundance Scan 886 (13.376 min): 03252.D (-) m/z 140.00 100.00% 140

5000 ------- 70 94 inn 13.00 13.20 13.40 13.60 13.80 0b ............... 1..... 84 108 .............. 1. ‘ I m/z 94.00 14.28% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089:2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 —,00) 13.00 13.20 13.40 13.60 13.80 54 68 m/ z 96.00 13.77% 80 95 108 121 ob 1 1 I ■ ' i 1 1 1 ' I 1 1 1 ' i ■ 1 1 1 i ‘ 1 1 1 i ' . | l......... ' i 1 ' 1 1 । 1 1 —L 111 m/z-> 30 40 50 60 70 80120 90 130 100 110 140 Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 82 13,00 13.20 13.40 13.60 13.80 5000 m/z 141.00 12.61%

54 68 96 | 111 0b / +TT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140 13.00 13.20 13.40 13.60 13.80 m/z 70.00 12.12%

5000

44 71 123 .I 86 96 112 ... I I I I I I I I I I । I I_ । । । । । 1 > । ■ I । । । । I 1 । 1 । I । । । TT ______ / 1 i ‘ 1 ■ ■ i ■ ■ ' 1 i ' mfe-> 301 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

)3252.D HP022102.M Mon Mar 04 12:33:55 2002 Page 8

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