GCMS analysis results for sample AE03248, March 2002

NYC 9/11 Public Portal Document ‘L MW

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 • Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 29900 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 56 2 2,5-Cyclohexadiene- 1,4-dione, 2,... 140 C6H404 000615-94-1 56 3 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 56 4 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 40 Abundance Scan 886 (13.376 min): 03248. D (-) m/z 140.00 100.00% 14.0

5000

70 . ......... . ................. 44 52 94 13.00 13.20 13.40 13.60 13.80 - — i Of ....... lal...... I. I ■. T’T m/z70.00 17.86% m/z-> :30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 "did N..... 13.00 13.20 13.40 13.60 13.80 54 68 m/ Z 94.00 13.40% 80 95 108 121 A

m/z-> 0 30 40 1' । ■ 50 60 III’’ 70 ana—.. 80 90 100 110 .... I I I...... +L rI 111 1 1' 1 1 1 I1 11 ' 1 1 1 120 130 140 Abundance #35123:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- 1-0 / 13.00 13.20 13.40 13.60 13.80 42 5000 m/ z 96.10 10.20% 69

53 84 94 112 01— "I'1'1.... I|. "" i 1t.F n/z-> 30 40 50 60 80 7090 100 110 120 130 140 Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 1-0 13.00 13.20 13.40 13.60 13.80 m/z 141.10 9.58%

5000 42 71 53 84 — 94 112 0- i ■ ■ ■ ■ i — I ' 1' ' r' ' 1 1 I ' 1 ' ' I ' 1 - rdz—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

J3248.D HP022102.M Mon Mar 04 12:33:28 2002 Page 11

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