GCMS analysis results for sample AE03248, March 2002

NYC 9/11 Public Portal Document Y DCaLII tpOulIU RCDOL L

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 ■ Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Decanal $$ n-Decaldehyde $$... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

13.59 0.05 ug/L 31873 Naphthalene-d8 13.20

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanal $$ n-Decaldehyde $$ n-De... 156 C10H20O 000112-31-2 53 2 Decanal (CAS) $$ n-Decanal $$ De... 156 C10H20O 000112-31-2 47 3 Decanal (CAS) $$ n-Decanal $$ De... 156 C10H20O 000112-31-2 45 4 Decanal 156 C10H20O 000112-31-2 38 Abundance Scan 905 (13.590 min): 03248.D (-) m/ z 43.10 100.00% 43 57

71 82 5000 136 |______ 49 13.20 13.40 13.60 13.80 14.00 0- i m/z 57.00 94.47% 1 1 i ■ ■ । ■ ■ ■ ' । ■ 1 ' ■ i ■ ■ 1 ' । 1 1 1 ‘ । ■ ■ ■ ■ । ■ 1 1 ' i ■ 1 Tl/Z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #55832: Decanal $$ n-Decaldehyde $$ n-Decanal $$ n-Decyl a... 43 57

5000 i 1 1 ■ ■ i ■ ' ■ ■ । । i ■ - 70 13.20 13.40 13.60 13.80 14.00 82 112 m/z 41.10 70.73% 95

m/z--> 0- ' ' i 40 50 60 ■ i ■ * 70 III... Ui... 1,.. 80 90 100 110 120 130 140 Abundance #55839: Decanal (CAS) $$ n-Decanal $$ Decyl aldehyde $$ De... 43 57

13.20 13.40 13.60 13.80 14.00 70 m/z 44.00 70.13% 5000 82

01 ' ' I' ' ■ i ■ ■ i ■ > n/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #55835: Decanal (CAS) $$ n-Decanal $$ Decyl aldehyde $$ De... 57 13.20 1340 13.60 13.80 14.00 m/Z 55.10 65.13%

5000 70 82 95 112

Tl/Z-> 0 1 1 i ' ■ ■ ■ i ■ ' 40 50 r i ' ' 60 70 80 ‘ 1* 90 100 -.'110I l. — 120 ,..... 130 140 13.20 13.40 13.60 13.80 14.00

)3248.D HP022102.M Mon Mar 04 12:33:28 2002 Page 12

NYC-WTC_000006161