GCMS analysis results for sample AE09335, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial : 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Decanal Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

13.83 0.24 ug/L 316597 Napthalene-d8 13.44

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanal 156 C10H20O 000112-31-2 64 2 Decanal 156 C10H20O 000112-31-2 64 3 Cyclohexane, 1,2-dimethyl-, cis- 112 C8H16 002207-01-4/43 4 2-Octene, (Z) -______________________ 112 C8H16 007642-04 30 Abundance Scan 1829 (13.826 min): 9335.D (-1816) (-) m/z 41.10 100.00% 41 57

70 5000 82 112 AA/AAA , NAAN h AAAA M AMAn 95 । i । l i 11^171 । I I । । । । i t j । I । 13.40 13.60 13.80 14.00 14.20 I । । । ' ' i । । । ■ । । । । । rr I, I । । । i‘ 4 I I I 1 1 I I | I I I ! | ! ! I ! 1’1’111111111111-11177717 m/ Z 57.10 94.49% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #108542: Decanal 41 57 29 5000 70 i 1 ' ■ ' i 1 1 82 13.40 13.60 13.80 14.00 14.20 m/ Z 43.15 89.51% 'I 95 112 TTTut r TTr 128 138 TWTON]

W I ‘' I m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4347: Decanal 43 wowW 57 । । । । । । । । । I । । CLBIU/I°I°I । । । 13.40 13.60 13.80 14.00 14.20 5000 29 m/ z 55.10 74.90% 70 82 II 95 112

m/z-> 10 r ■ i ■ 15 r i1

20 30 IT 40 J i l . . A... 128 138 155 60 70 80 90 100 110 120 130 140 150 160 ' ■ i 11 1 1 i '' ‘11 ■' '1 i1 1 ' ■ i ''

Abundance #111705: Cyclohexane, 1,2-dimethyl-, cis- 55 44— A ' 1 I 1 1 ■ 1 i ' ■ ' ' i ■ ■ 13.40 13.60 13.80 14.00 14.20 A m/z 70.10 55.77% 97 41 5000 83 70 112 27 i r j-' । I । । । i । I [ L i । |1JI 1 1 i 1 ' 163l— ' i '1 1' I T1 । । । > > । । i i । । < । । If । r r r। i r ___________ __________ }U’ I I I I I I I [ l I I I J I I IUP"

Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 13.40 13.60 13.80 14.00 14.20

9335 .D 050102.M Mon May 06 13:59:47 2002 Page 11

NYC-WTC_000044686