GCMS analysis results for sample AE09335, May 2002

NYC 9/11 Public Portal Document

Data File C : \MSDCHEM\ 1 \DATA\ 050202\9335.D Vial: 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Phenanthrene, 9-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.42 ug/L 600836 Phenanthranene- dl 0 22.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 40/ 3 Isoquinoline, 1,2,3,4-tetrahydro... 328 C18H20N2O4 1000128-79-2 40 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2/40 Abundance Scan 3319 (22.580 min): 9335. D (-3312) (-) m/z 192.10 102.00* 102

5000

92 96 146160 _ ....... I ' I ' ’ ' ' I 1 ' ' ' I 22.20 22.40 22.60 22.80 23.00 A Tri TPH 40 66 82 ,1 118 I I q-thhyllthr"d00/1"7 i i 1‘ । i । । | 11 I I "| I I i r । i i 1 i ■ 1 1 1 r ' 1 1 i 1 1 • ri Ttt’’ m/z 191.00 22.31% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #81033: Phenanthrene, 9-methyl- 192 ’ 1 i ' 1 / 1

5000 1 j I I I I I I I I I I I I

22.20 22.40 22.60 22.80 23.00 m/z 193.10 15.72% 96 165 i 39 63 82 1115 139 | l r i i । । i'i ( । i i । i'T i I । i i r' i । TT I k I II * । T i i 1 | i i ' i 1 1 ■ 1 r ■ ■' r 1 ' ■ i' ''' i' ' ■ ■ i ■ ■1' i 1 '' ■ i /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #81041: Phenanthrene, 3-methyl- 102 ..... n...., 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 14.75%

96 IRS 1

39 63 82 ,115 150 P t...... 111101 1 i r I | 3 i I n | ■ T ( | | I ill | I | i I | I || i | T | i 1 | i TT I | 1 > > i | I

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #81065: Isoquinoline, 1,2,3,4-tetrahydro-1-[2-nitrobenzyl]... TT A TI .... ... ' 1 1 1 ' ' 1 1 1 192 22.20 22.40 22.60 22.80 23.00 m/ z 96.10 14.74%

5000

176 49 63 78 1 04 . 131 148162 | _ 207 236250264 280295311 328 __ ________ _i I _______ . .| । i i । i । i i ' i । । ' i । r । । i । । r । । । T । । । I । ■ । f । । I । rr41 < | 17 < । | r i r t | i'>-r i“| I i i i | i i i r | । i i > | i I i r | | i i i I tr I '"I- । । r — —y 1" 1" I r~~

n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 1 22.20 22.40 22.60 22.80 23.00

9335.D 050102.M Mon May 06 13:59:48 2002 Page 12

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