GCMS analysis results for sample AE09335, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial: 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phenanthrene-dlO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.58 ug/L 823975 Phenanthranene-dl0 22.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 93 3 Cyclohept anone, 4 -phenyl- 188 C13H160 067688-28-2 50 4 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 40 Abundance Scan 3409 (23.109 min): 9335. D (-3402) (-) m/z 188.20 100.00% 188

5000

1 1 । 1 1 1 I Onv I I I I I I I 80 94 22.80 23.00 23.20 23.40

m/z-> 40 54 i । < r। i । i i । i । i i i i | ( । > i । f l'r 66 jI....... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TTT ।1"11 132,146 140170 — m/z 189.20 15.41% Abundance #79827: Phenanthrene-d10 188

5000 ■ ■ i 1 1 22.80 23.00 23.20 23.40 m/z 94.10 14.97% 80 94 160 30 42 52 66 1 108 118 132 146 ,|,| 170179,1,1 | 11" " l " " 11 "11' 1" 1111111' 11 ■ । " 11111] I I । i | 1 111 [ । 11 i [ 1 11 । pl r 1 । । । । 11 11 rH'l1! । 11 p i 11 । itPI'i i r TTl m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 1 1 i ■ ' — —— — — 22.80 23.00 23.20 23.40 5000 m/ z 80.10 13.30%

80 94 160 66 108 118 132 146 || . .................. , 17 30 42 52 11 I I I ■ [ I I >■ I I ■ I ■ ■ I I 1 I I I I I I I . .......... I I I 1 p I ftp I I I p I I I p I I l p I "TT‘ I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ............. ..................................... Abundance #79739: Cycloheptanone, 4-phenyl- ' 1 I ' ' ' ' 1 1 ' 1 1 1 ' ' 1 1 1 1 ' I 188 22.80 23.00 23.20 23.40 117 m/z 184.10 12.42% 104 91 160 5000 131 170 27 39 51 65 78 145

m/z-> 1111.11111,11, 11 l । Alp m m r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 + 1| ' ' l 1 22.80 23.00 23.20 23.40 1 1 1 1 1 ' I ' ' 1 1 I

9335.D 050102.M Mon May 06 13:59:49 2002 Page 13

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