GCMS analysis results for sample AE09336, May 2002

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Laboratory report documenting GCMS analysis of sample AE09336 conducted on May 8, 2002.

NYC-WTC_000044708–000044722

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\050202\9336.D Vial: 14 Acq On 2 May 2002 10:16 pm Operator: Mclean Sample 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.56 ug/L 614404 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 87 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 39 4 Pentacyclo[8.4.0.0(3,7) .0 (4,14) . . . . 188 C14H20 1000099-27-2 36 Abundance Scan 3409 (23.109 min): 9336.D (-3403) (-) m/z 188.20 100.00% 188

5000 T > I ' — I I I — , I 1 — I I I I I > r 80 94 22.80 23.00 23.20 23.40 42 52 66 ,|| .... 132 158 .. ^1 | I > r । । i । i i । ill I | I'l t i | I I I ’| | i I I i | I i I I' < r I > j I I i i । ■ i । i । । KI i | । > i > | I । ■ i | i । i । | i < I I'| i । i i | i > m/z 189.10 15.67% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

......../....................... 5000 ' 1 । 1 1 1 ■ r ■ 11 ■ । 1 ■ 1 ■ । ■ ' 1 1 । 22.80 23.00 23.20 23.40

80 m/z 184.10 15.46% 94 160 30 42 52 66 । । । । । । । i't। । । । । i i 11 i > । 11 l~i i । i I I i । i > il i । । 11 +108,118.132.146—4179179/ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 ■ ■ i 1 22.80 23.00 23.20 23.40 5000 m/z 80.05 14.62%

RR 80 94 160 170179, I m/z-> 17 30 42 52 0 108 118 132 146 1 n | | I I I | | I I I i । I i ! I [ I I i I | 1 I I I | | rfl I | i i I | H I I [ i i I I I i i i I I I i i I |t I I TTMTT t I rPI‘1 | | i ttri I'rP 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 4 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )]tetradeca... ... I ' ' I ' ' 1 ' 1-1 1 1 1 1 ' I ' 1 ' ' I 188 22.80 23.00 23.20 23.40 m/ z 94.05 12.88%

5000 79 91 55 67 1 105 117 131 n/z-> sMalsyall 444- — । । । । r। । i । । । । r। < । [ । HH+ 145.158173 . Il 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ll ' 11'1111 r'111 ■ ‘11'1 H I''1111,11 1 I I I I I ’ [ I I f 1 ] I I I I I I I I I r 22.80 23.00 23.20 23.40

9336.D 050102.M Tue May 07 12:07:24 2002 Page 8

NYC-WTC_000044720

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NYC-WTC_000044720Source: NYC Law Department, mirrored locally

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