GCMS analysis results for sample AE10134, May 8 2002

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Laboratory report documenting GCMS analysis of sample AE10134 conducted on May 8, 2002.

NYC-WTC_000044408–000044429

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

'Data File C:\MSDCHEM\1\DATA\050202\10134.D Vial : 26 Acq On 3 May 2002 9:42 am Operator: Mclean Sample 4/29 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 10 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.54 ug/L 428487 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 86 3 Pentacyclo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 39 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 Abundance Scan 3409 (23.109 min): 10134.D (-3403) (-) m/z 188.10 100.00% 188

5000

80 94 156 22.80 23.00 23.20 23.40 41 54 71 .| I । i ii i । r Pr i~| r )' I i p I i i । i I i I | I i I i । 'i i I I p i i i p I i i । 111111" 1' i i' l H-m m/z 189.20 18.56% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 • • l ■ > ■ > 1 ' 1 -I • l • - 1 ' I ' • • 1 I 22.80 23.00 23.20 23.40 m/z 80.05 13.43% KA 80 94 160 , 1 17 30 42 52 0 J J 108 118 132 146 1 170179, ‘p-rrr !i । i i i i । i i i T1 ] । i i i p i । i p t 11 । 1 I I । । i rl'I p rr t p I i rp I । I | । i । । । rri'rpt ’Ti'|"i i_t'।'। r i I’l'l'i i i i । i i > r p11 I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ..... pi................... Til | I Ti ■ p i i I i | I I i i | i i i i |

22.80 23.00 23.20 23.40 5000 m/z 184.10 12.13%

80 94 160 42 52 i । t 66 30 । , il 108 118 132i t I I i । i! |-I 1 i 1 ! | I I i r| I IFI7 i i i 1 [ i i i i i । i k < i । i i > i । i i i > p i ■ ■ । H i 146,44170179 — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12) 0(2,7).0(6,11)]tetradeca... ‘ I’* I 1 1 1 1 I 1 1 1 ' I 188 22.80 23.00 23.20 23.40 m/ z 94.05 11.61%

5000 79 91 55 67 105 105 117 131

m/z-> TT mllJ U 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 +1510.173 ., ' 1 1 22.80 23.00 23.20 23.40

10134.D 050102.M Mon May 06 12:24:17 2002 Page 13

NYC-WTC_000044424

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NYC-WTC_000044424Source: NYC Law Department, mirrored locally

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