GCMS analysis results for sample AE10134, May 8 2002

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Laboratory report documenting GCMS analysis of sample AE10134 conducted on May 8, 2002.

NYC-WTC_000044408–000044429

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

'Data File C:\MSDCHEM\1\DATA\050202\10134.D Vial : 26 Acq On 3 May 2002 9:42 am Operator: Mclean Sample 4/29 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 2-Propen-1-one, 1-(2-hydrox... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

30.98 0.27 ug/L 175660 Chrysene-dl2 30.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propen-1-one, 1-(2-hydroxyphen... 238 C16H14O2 016635-14-6 22 2 Benzaldehyde, 4-methoxy-, (pheny... 238 C15H14N2O 001149-69-5 18 3 9-Fluorenone-l-carboxylic acid, ... 238 C15H10O3 005406-90-6 12 4 2-Phenazinecarboxylic acid, meth... 238 C14H10N2O2 018450-12-9 9 Abundance Scan 4748 (30.977 min): 10134.D (-4747) (-) m/z RvvyWyA" 40.10 100.00% 40 84 207 238 104 116 5000

30.60 30.80 31.00 31.20 31.40 1 । 1 1 TT II" 1 1 1 1 ' ' 1 i ’ 1 1 1 i 1 ' ' 1 i 1 ' ' ' i 1 1 1 1 1 1 1 m/z 2 06.90 92.80% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #91004: 2-Propen-1-one, 1-(2-hydroxyphenyl)-3-(4-methylphe... 238 118 147 A M A,Ar YA,M/WAMMAWyWNY"YWW 5000 30.60 30.80 31.00 31.20 31.40 65 223 m/z 84.00 87.12% 91 105 ।

n/z-> 20 nil 39 — I 51 i ■ ■ i ■ .

40 ■

60 80 77 All.. 100 120 140 II 165 — ————— 1 ■ i 1 1 1 1 i 1 1 160 180 200 220 240

IAMr Abundance #91005: Benzaldehyde, 4-methoxy-, (phenylmethylene)hydrazone 2318 11/ 30.60 30.80 31.00 31.20 31.40 5000 92 131 m/z 238.10 75.76% 161 77 । 103 208 39 51 65 120 — " 1 'll. , ill,,. —lu—L T"IT 180 1 I1' 1 ' 1 1 ' 1 1 ■ । ' II223 — ' 1 i 1 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #84914: 9-Fluorenone-1 -carboxylic acid, methyl ester 1 i 1 1 1 _i ■ ■ ■ ■ ■ । r • ■ ■ i ■ ■ 207 30.60 30.80 31.00 31.20 31.40 238 151 m/ z 104.00 68.94%

5000 180 75 31 163.187 87 I?4 125 139 .165 . 195 i ' 1 1 । 1 ■ 1 1 । 1 ■ ■ 1 । ' — 1—— ' 'i"i 1 1 " n 1" ITt 1 'I' ' 1 i 1 223 11 1 ' I 1 1 ' rLU. m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 30.60 30.80 31.00 31.20 31.40

10134.D 050102.M Mon May 06 12:24:18 2002 Page 14

NYC-WTC_000044425

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