GCMS blank analysis results, sample AE10809, May 2002

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Data File : C:\MSDCHEM\1\DATA\051402\0507LB.D Vial: 16 Acq On : 15 May 2002 2:34 am Operator: Mclean Sample : 5/7 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 2-Propenoic acid, 3-(3,4-di... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 36.48 2.12 ug/L 966113 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenoic acid, 3-(3,4-dimetho. .. 222 C12H1404 005396-64-5 22 2 3-Acetyl-1-(4-chlorophenyl)-5-me... 265 C12H12C1N3O2 1000210-17-3 9 3 2-Propenoic acid, 3-(3,4-dimetho... 222 C12H1404 005396-64-5 9 4 2H-l-Benzopyran-3-carboxylic aci... 400 C26H2404 019723-39-8 9 Abundance Scan 5684 (36.476 min): 0507LB.D (-5683) (-) m/z 222.10 100.00% 222

75 327 355 5000 191 265 148 429 36.20 36.40 36.60 36.80 0- I m/z 207.05 64.00% m/z-> 50 100 150 200 250 300 350 400 Abundance #88141: 2-Propenoic acid, 3-(3,4-dimethoxyphenyl)-, methyl... 222 wu"wpt 5000 191 1 ' i ' 1 36.20 36.40 36.60 36.80 m/z 355.00 55.56%

0 , , r„51L ,477 2—9,4 A147 1, 4---- Ti ' m/z-> 50 100 150 200 250 300 350 400 Abundance #9660: 3-Acetyl-1-(4-chlorophenyl)-5-methyl-4,5-dihydro-1 H... 43 222 "A- 36.20 36.40 36.60 36.80 5000 m/ z 75.00 52.89% 265 125 I 153 180 63 T 01 +-,4444,4+123.4200- 1 l ' 1 i ■ /z-> 50 100 150 200 250 300 350 400 Abundance #126976: 2-Propenoic acid, 3-(3,4-dimethoxyphenyl)-, methy... ■ ■ i ■ > 1 i 1 ' 1 ■ i ■ ' 222 36.20 36.40 36.60 36.80 m/z 326.80 52.00%

5000 191

. 51 77 119 147 0 24 14 96, 4 ,1^1 179 . 1 T—l ' TRl 1 i ' ■ ' i 1 1 ' 1 i m/z-> 50 100 150 200 250 300 350 400 36.20 36.40 36.60 36.80

0507LB.D 050102.M Thu May 16 12:36:03 2002 Page 21

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