GCMS analysis results for sample AE10811, May 2002

NYC 9/11 Public Portal Document

.Data File : C:\MSDCHEM\1\DATA\051402\10811.D Vial : 21 Acq On : 15 May 2002 6:39 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Benzene, 1-(1-cyclohexen-l-... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.48 ug/L 628249 Phenanthranene- dl 0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1-(1-cyclohexen-l-yl)-4.. 188 C13H160 020758-60-5 58 2 Antipyrine 188 C11H12N2O 000060-80-0 53 3 Antipyrine 188 C11H12N2O 000060-80-0 53 4 Antipyrine 188 C11H12N2O 000060-80-0 53 Abundance Scan 3409 (23.109 min): 10811 .D (-3402) (-) m/z 188.15 100.00% 188

5000

94 ____ I | | Ir _________________ I i I i i ] I | I iI kl | i > T

43 57 66 80 124132 146 160 22.80 23.00 23.20 23.40 01 ----- 'I.............I i i'| •/r, ■> |’i t t ।-| i i rr|ri r m/z 94.05 20.85% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 188

5000 160 I-1 I * I I I J I 15 I I I I I Ipn——p"t"j 22.80 23.00 23.20 23.40 — 173 m/z 189.15 13.40% 1115 129

m/z-> Ol TT

Abundance 20 41 51 65 77 . 91 | 102 8 l| I । । ll , t pv 11 ililps 11 nlllj- । rt । rlt-- millipti 11 H— — 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 145 AL #125688: Antipyrine 188 / 96 22.80 23.00 23.20 23.40 5000 77 m/z 184.10 10.47% 56 105 39 27 64 ill | 115 129 145 159 173 li ol ‘i‘3 pelgousyhun । i-I'I-i 11 ill pi 111 '|-i 11111 i'i 111,11'|,' 11111'' 11' 111 mi

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ........ \................................... Abundance #79725: Antipyrine 1 ' I ' 1 1 1 T । । 1 ' T"1"'1 I’IIIII 188 22.80 23.00 23.20 23.40 m/z 187.15 9.86% 96

5000 77 56 105 39 67 / 115 130 145 159 173 27 0 nguvenyun -Tp I j l Hl ' | I I I I 1 1 M/tvrg-t’l j I i i 1*1 t'l j'l । I i | | > | i i i tbp-r I r IL 111 m-n I |'! I I I | I I I ! |

/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10811.D 050102.M Thu May 16 14:13:32 2002 Page 2 0

NYC-WTC_000046060