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GCMS analysis results for sample AE09574, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09574 conducted on May 14, 2002.

NYC-WTC_000023107–000023121

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document . Data File C:\MSDCHEM\l\DATA\050902\9574.D Vial: 10 Acq On 9 May 2002 10:37 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.48 ug/L 724973 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 2 Phenanthrene-diO 3 Selenide, ethyl 1-methyl-1-pente... 188 188 188 C14D10 C14D10 C8H12Se 001719-06-8 72 001517-22-2 64 4 025128-48-7 50 Q 4 Antipyrine 188 C11H12N2O 000060-80-0 49 Abundance Scan 3409 (23.109 min): 9574.D (-3402) (-) m/z 188.10 100.00% 1(18

5000

80 94 -------- 160 22.80 23.00 23.20 23.40 44 57 66 . ■ 111 pl 1111111 — m/z-> 0 H "11111" i1"11'11'1111’I’ । ■ 11 ■ i'" 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ,1117113. m/z 94.10 20.76% Abundance #79826: Anthracene-d10- 1(8

5000 ■ ■ i ' ■ 22.80 23.00 23.20 23.40 m/z 80.10 16.17% 17 30 42 52 ee 0 80 , 94 , 108 118 132 160 146 11) 170179 ,, 0 H ■ " 1 | ' r 1 •' ' | ' ' 1 ' | 1 1 ‘ ' | ■ 1 I 1 | " 1 1 1 1 ' ' th . | I ... | I 1 . 1 | I I IT] I 1 | . I ll , I 1 l’l’l" I I I | I I I I r’l’l i , ‘I m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(8 .....................................................

22.80 23.00 23.20 23.40 5000 m/z 184.10 13.52%

80 94 160 30 42 52 66 0 —mmTTTHTTTH 11111111"108 118 132 146 .J 170179/ ■ I" " I"1111" 11111 ‘ ।1'I'l I'1"111111111111" । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 188 22.80 23.00 23.20 23.40 m/z 189.20 13.52%

5000

79 159 145 173 91 107 119 131 ,| 0 1 '1 "" I" " I" " I" " I " 1' I " ‘ TWTTTUTTTTTTTTTTTTTTTT ll 1’1 ... / , .......... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9574.D 050102.M Mon May 13 11:49:49 2002 Page 8

NYC-WTC_000023119

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NYC-WTC_000023119Source: NYC Law Department, mirrored locally

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