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GCMS analysis results for sample AE09574, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09574 conducted on May 14, 2002.

NYC-WTC_000023107–000023121

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023118
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

• Data File C:\MSDCHEM\l\DATA\050902\9574.D Vial: 10 Acq On 9 May 2002 10:37 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Thiocyanic acid, 2-benzothi... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.34 ug/L 510759 Phenanthranene- dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59/ 2 Bitoscanate 192 C8H4N2S2 004044-65-9 58 3 Bitoscanate 192 C8H4N2S2 004044-65-9 58 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-/ 45 Abundance Scan 3319 (22.580 min): 9574.D (-3311) (-) m/z 192.10 100.00% 192

5000

62 96 146 160 22.20 22.40 22.60 22.80 23.00 46 70 82 | 118 | 0- TTWTTTTTTTTTTTTHTTT ■ 111 i 1111 ■ 111! 1111111111 TDWTTTTTHTP m/z 191.10 18.65% niz-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

5000 .... 0 22.20 22.40 22.60 22.80 23.00 m/z 146.10 13.73% 69 0 108 134 148 160 /z-> 45 1...1.8... I. 122 I 0- "I".. ................... 1.......... THTTTTTTHTTTTTT ‘ ‘I’’ 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125827: Bitoscanate 192 ------A . i . ... 1 . 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.00 11.80% 134 90 160 50 63 75 4 14 0 '' I"'' I'1 ‘' I'28.4444 192.116 „ . 148 1++ **r’ Ir.. i. |'i.. 11 i'I'i . ।. > r.... " i" " i" " i "i” nfe-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125828: Bitoscanate ,...... 11 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 11.40%

5000 134 63 160 50 .. 50 63 75 90 102 75 122 148 176 0-TTTm i i pt 4+ rll. -ll [I1! r r । It Ir 111TT TTTTtrTH TTp-r ft............. ._ i . ■ . ■ i ■ ■ i . 1 i ■ ■ ' 1 i ■ ■ n/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 22.20 22.40 22.60 22.80 23.00

9574.D 050102.M Mon May 13 11:49:49 2002 Page 7

NYC-WTC_000023118

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NYC-WTC_000023118Source: NYC Law Department, mirrored locally

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