GCMS analysis results for sample AE09334, May 2002

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Laboratory report documenting GCMS analysis of sample AE09334 conducted on May 8, 2002.

NYC-WTC_000044657–000044671

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document X ‘ ‘L

Data File C:\MSDCHEM\1\DATA\050202\9334.D Vial : 12 Acq On 2 May 2002 8:38 pm Operator: Mclean Sample 4/29 Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C : \DATABASE\NIST98 . L ********************************************************************* Peak Number 5 Thiocyanic acid, 2-benzothi... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.35 ug/L 357772 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53/ 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 3 5H-Tetrazole-5-thione, 1,4-dihyd... 192 C8H8N4S 1000142-22-5 40 4 1,5-Naphthalenedithiole 192 C1OH8S2 1000223-6945 38 Abundance Scan 3319 (22.580 min): 9334. D (-3312) (-) m/z 192.10 10b.00% 192

5000

40 82 96 146 160 ..... ..... A 22.20 22.40 22.60 22.80 23.00 52 “ aonain, 1 r '1' r 11' 111 111 .......... 120 70 11'1111'11111111'11111 11■■■।■ TTrt ।| ■ ■ ■ ■ । + m/z 191.10 19.16% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 14.16% 69 4 no 13A 45 । | 82 90 100 122 1 148 160 ........... I'" TIPTPTTTTTTTTTTTTT m/z-> 30 40 !50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 ..................A............. / 161 ~1 । 1 ■ 1 ‘ i ' 1 1 ■ । 1 1 ' 1 । 1 1 1 1 । 1 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 12.87%

77 91 . 121 149 177 A .............. .52 ........................ I 103 I 138 I 1 mll I I | I I I I — ! > | |l ! I | I , I 1 I I I | I I I I I I I I I I I I I I I I I I I > I I I I I I I I I I UI 1 1 i ' 1 ' 1 i 1 ■ 1 ■ i TI11 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80933: 5H-Tetrazole-5-thione, 1,4-dihydro-1-methyl-4-phenyl- 135 192 22.20 22.40 22.60 22.80 23.00 m/z 96.10 10.63% 77 5000 51 61 91I . 123 39 104 1111 rlrpl 11 + TTT1,6940/011/7/2841/1 TT 149 163 TTuTmmT |, HL I [ r i i i [ ' i — j , i i | i r

/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9334.D 050102.M Mon May 06 13:58:39 2002 Page 8

NYC-WTC_000044668

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