GCMS analysis results for sample AE09334, May 2002

NYC 9/11 Public Portal Document LpUL —SpW

Data File C:\MSDCHEM\1\DATA\050202\9334.D Vial: 12 Acq On 2 May 2002 8:38 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.48 ug/L 486216 Phenanthranene-dlO 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Pentacyclo[8.4.0.0(3,7) .0 (4,14) . . . . 188 C14H20 1000099-27-2 36 Abundance Scan 3409 (23.109 min): 9334.D (-3403) (-) m/z 188.10 100.00% 188

5000 ----- 80 94 160 22.80 23.00 23.20 23.40 < II ! |l।I !| I। I।| 41 66 । । i । i । । I i-i I ] । । । i । । i । । । i । i । । i I I । | । i I t 132 'I""i I rill | rm |-r i i i | ra 111TTT m/z 189.20 18.17% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188

......... /............................ 5000 1 । } I rm । | । । । । । । । । । ] II ii [

22.80 23.00 23.20 23.40 m/z 94.05 16.48% KA 80 94 160 , । 17 30 42 52 00 I . 108 118 132 'l I I I I I I I I I I I I t’rrrtr I I'l I I I I'l I I I I I I I I I I I I I I I I I I I [ t I 1'1 TFTTTTTTTTT 146, .,179179., TI TT mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 80.05 14.27%

80 g4 160 ; 30 42 52 66 . . 11 108 118 132 I | I146 I, 170179,|,| | I i'll ' I I I I II ] ill rptt I I I I I I tj r l I r , 1 i rl i i i f | I I i i | I i i i । i i i i । i rrij Iti I 1 I | I lM‘1‘11! 1 1 T | 1 I ! I | |lllll|l| I I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 - Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z 184.10 12.70% 145 5000

117

m/z-> ' i " " r 1" r 41 51 63 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 77 89 102 130 - 159 '73 I 1 I | I I <

22.80 23.00 23.20 23.40 । | I ! “I ■ | I I I I | —! — r

9334.D 050102.M Mon May 06 13:58:40 2002 Page 9

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