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GCMS analysis results for sample AE09575, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09575 conducted on May 14, 2002.

NYC-WTC_000023130–000023147

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023141
OCR text

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NYC 9/11 Public Portal Document

. Data File C:\MSDCHEM\l\DATA\050902\9575.D Vial: 11 Acq On 9 May 2002 11:26 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.55 ug/L 884880 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 53 4 4-Fluoro-6-methyl-2-phenylpyrimi ... 188 C11H9FN2 051421-92-2 50 Abundance Scan 3409 (23.109 min): 9575.D (-3402) (-) m/z 188.15 100.00%| 188

5000

1 ■ i ■ ' ■ ' । ■ i 1 1 1 ' i 43 57 66 132 146 158 |, 80 22.80 23.00 23.20 23.40 0 1' ! । 'P ----- TIWWTPTTTTTTTTTTTTTTTTH m/z 189.15 19.95% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/ z 184.10 14.47%| „ 80 94 160 । 17 30 42 52 0 | | 108 118 132 146 |L| J I170179, | 0 ^‘1 I I I | I I I I [' t J J I | I I I I | I I 1 ! | t'l I I | I 1 1 I | tl Tt | I I M | ! I I I | I U 1 | 1 I I I ] I I I I | I | I I | I | I | I I J l ] "’l’l’t I I J 11 iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 94.00 13.04%

94 160 80 30 11 42 52 66 108 118 132 146 II. 1701791,1 0 TmPPTmOTTOTTTTTTTHTHTTTTT ‘I n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- 188 22.80 23.00 23.20 23.40 117 m/ z 80.10 104 12.3 9%| 91 160 5000 131 170 145

/z-> . 1 —llHHH++ 0 1111111111 * 11 27 39 51 65 78

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 , ,I | | TI’’ -rp-r U 22.80 23.00 23.20 23.40

9575.D 050102.M Mon May 13 11:51:00 2002 Page 7

NYC-WTC_000023141

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NYC-WTC_000023141Source: NYC Law Department, mirrored locally

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