GCMS analysis results for sample AE09334, May 2002

NYC 9/11 Public Portal Document ‘ ‘L

Data File C:\MSDCHEM\l\DATA\050202\9334.D Vial: 12 Acq On 2 May 2002 8:38 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Diftalone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.90 0.37 ug/L 283322 Perylene-dl2 34.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Diftalone 264 C16H12N2O2 021626-89-1 43 2 Diftalone 264 C16H12N2O2 021626-89-1 37 3 N-Acetyltranylcypromine 175 C11H13NO 078682-61-8/16 41-Phenyl-1,2,3,4-tetrahydroisoqu...209C15H15N 022990-19-8 9 Abundance Scan 5416 (34.901 min): 9334. D (-5415) (-) m/z 131.80 100.00% 40 132 ft

264 5000 84 191 209 118 34.60 34.80 35.00 35.20 ■ 1 i ' 1 m/ z 40.10 84.60% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #122112: Diftalone 132

264

5000 90 34.60 34.80 35.00 35.20 105118 m/z 264.20 57.70% 77 51 63 1,1 j li , J. . ________ 235 h ___________________ ll 1,1 II I ' ’ 1 fL" I I > I > I I I I L—— " ] I — I I I I I 1 "I I I 1 1 I I I I III" I I I —

n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59855: Diftalone 132 264 ■ 1 i ■ ' 1 1 i 1 ■ ' ■ i ' 1 1 1 i ' 1 1 ■ i 34.60 34.80 35.00 35.20 5000 m/z 128.00 41.19% 90 105118

m/z-> 18 1 1T|i~i।ni।|r1ii।ir

20 39 51 63 77

40 .1 _

60 I_ _ .III

80 , I | A100 120 1................ 178........ 208........................ || 140 160 180 200 220 240 260 Abundance #59666: N-Acetyltranylcypromine 1 ■ i 1 ■ 1 ■ i~ 111*1‘III+‘I 132 34.60 34.80 35.00 35.20 m/ Z 36.00 37.48% 116 5000 60 84

103

m/z~> 20 40 60 ■ ■ i 80 LL 100 120 140 146 160 175 180 200 220 240 260 II I Vi । 1 1 1 T 1 1 34.60 34.80 35.00 35.20 W

9334.D 050102.M Mon May 06 13:58:43 2002 Page 10

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